4-[2-(5-乙基-2-吡啶基)乙氧基]苯甲醛合成路线 (共 16 条)
参考文献
Takeda Chemical Industries, Ltd.
Patent: US5554758 A1, 1996 ;
反应条件
piperidine in ethanol 5 h; Heating / reflux;
参考文献
RICHTER GEDEON VEGYESZETI GYAR RT.
Patent: WO2005/58827 A1, 2005 ;
Location in patent: Page/Page column 11-12 ;
反应条件
1: 64 percent / piperidine / ethanol / Heating 2: 65 percent / hydrogen / Pd-black / dimethylformamide / 5 h / 50 °C View Scheme
参考文献
Mohanty, Sandeep; Reddy. G, Sandeep; Karmakar, Arun Chandra
Letters in Organic Chemistry, 2014 , vol. 11, # 3 p. 197 - 202
反应条件
pyrrolidine in methanol T=10 - 50°C; 8 h;
参考文献
SANDOZ AG
Patent: WO2005/49610 A1, 2005 ;
Location in patent: Page/Page column 16 ;
参考文献
Takeda Chemical Industries, Ltd.
Patent: EP257781 B1, 1991 ;
反应条件
1: sodium hydrogensulfite / water; hexane 2: trichlorophosphate / toluene / 8 h / |Reflux View Scheme
参考文献
Mohanty, Sandeep; Reddy. G, Sandeep; Karmakar, Arun Chandra
Letters in Organic Chemistry, 2014 , vol. 11, # 3 p. 197 - 202