4-甲氧基苯基磷酸二乙酯合成路线 （共 39 条）
反应条件
copper(l) iodide; caesium carbonate in ethylene glycol dimethyl ether T=80°C; 2 h; Inert atmosphere;
参考文献
Miao, Wenjun; Gao, Yuzhen; Li, Xueqin; Gao, Yuxing; Tang, Guo; Zhao, Yufen
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 14-15 p. 2659 - 2664
参考文献
Yang, Jie; Liu, Guo-Yun; Lu, Dong-Liang; Dai, Fang; Qian, Yi-Ping; Jin, Xiao-Ling; Zhou, Bo
Chemistry - A European Journal, 2010 , vol. 16, # 43 p. 12808 - 12813
参考文献
Hoechst Aktiengesellschaft
Patent: US5242908 A1, 1993 ;
反应条件
1: C5H12IO3PZn With [RhCl(η2:η2-cycloocta-1,5-diene)]2; 1,1'-bis(diphenylphosphino)ferrocene in tetrahydrofuran 0.0833333 h; Inert atmosphere; 2: para-iodoanisole in tetrahydrofuran T=60°C; Negishi coupling reaction; 10 h; Inert atmosphere;
参考文献
Takahashi, Hideki; Inagaki, Shinya; Yoshii, Naoko; Gao, Fuxing; Nishihara, Yasushi; Takagi, Kentaro
Journal of Organic Chemistry, 2009 , vol. 74, # 7 p. 2794 - 2797
反应条件
[2,2']bipyridinyl; copper (II) acetate monohydrate; potassium carbonate in dimethyl sulfoxide T=110°C; 4 h;
参考文献
Rout, Laxmidhar; Regati, Sridhar; Zhao, Cong-Gui
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 18 p. 3340 - 3346
反应条件
zinc(II) iodide in tetrahydrofuran 12 h; Inert atmosphereReflux;
参考文献
Richardson, Rebekah M.; Wiemer, David F.
Organic Syntheses, 2013 , vol. 90, p. 145 - 152
反应条件
1: NBS; AIBN / CCl4 / Irradiation 2: Heating View Scheme
参考文献
Journal of the American Chemical Society, , vol. 129, # 27 p. 8443 - 8457
反应条件
1.1: NaH / tetrahydrofuran / 25 °C 1.2: tetrahydrofuran / 20 °C 2.1: NBS; AIBN / CCl4 / Irradiation 3.1: Heating View Scheme
参考文献
Journal of the American Chemical Society, , vol. 129, # 27 p. 8443 - 8457
反应条件
1: 89 percent / PBr3 / diethyl ether / 2 h / 20 °C 2: 95 percent / 5 h / Heating View Scheme
参考文献
Organic Letters, , vol. 8, # 25 p. 5833 - 5836
反应条件
water; palladium diacetate; N-ethyl-N,N-diisopropylamine; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in tetrahydrofuran 2 h; Inert atmosphereReflux;
参考文献
Laven, Gaston; Stawinski, Jacek
Synlett, 2009 , # 2 p. 225 - 228
