1147550-11-5合成路线 (共 743 条)
反应条件
beim Erhitzen auf dem Wasserbad;
参考文献
Johnson; Hill; Bailey
Journal of the American Chemical Society, vol. 37, p. 2415
反应条件
in water; benzene T=50°C; 2 h;
参考文献
Allakhverdiev; Alekperov; Shirinova; Akperov
Russian Journal of Organic Chemistry, 2000 , vol. 36, # 4 p. 565 - 567
反应条件
1.) Me2CO, 40 deg C, 30 min, 2.) Me2CO, 20 deg C, 2 h; Yield given. Multistep reaction;
参考文献
Brindley, Jocelyn C.; Caldwell, Jennifer M.; Meakins, G. Denis; Plackett, Simon J.; Price, Susan J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 1153 - 1158
参考文献
Veszpremi, Tamas; Barta, Istvan; Nagy, Jozsef
Acta Chimica Hungarica, 1986 , vol. 122, # 3-4 p. 243 - 250
反应条件
hydrogenchloride in water T=100°C; 16 h;
参考文献
WO2009/114552 A1, ;
Page/Page column 94-95 ;
反应条件
bromine; triphenylphosphine in acetonitrile T=20°C; Thiocyanation;
参考文献
Journal of Chemical Research - Part S, , # 11 p. 676 - 677
反应条件
1: ammonium thiocyanate With APDPP; bromine in acetonitrile T=20°C; 2 h; 2: diphenylmethanol in acetonitrile T=20°C; 3 h;
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 184, # 8 p. 2010 - 2019
反应条件
1: ammonium thiocyanate With APDPP; bromine in acetonitrile T=20°C; 2 h; 2: Ph-CH(OTMS)-Ph in acetonitrile T=20°C; 0.0833333 h;
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 184, # 8 p. 2010 - 2019
反应条件
1: ammonium thiocyanate With bromine; triphenylphosphine in acetonitrile T=20°C; Addition; 2: Ph-CH(OTMS)-Ph in acetonitrile T=20°C; Substitution;
参考文献
Synlett, , # 1 p. 65 - 66
反应条件
1: ammonium thiocyanate With bromine; triphenylphosphine in acetonitrile T=20°C; Addition; 2: Benzhydryloxy-tert-butyl-dimethyl-silane in acetonitrile T=20°C; Substitution;
参考文献
Synlett, , # 1 p. 65 - 66