1147550-11-5合成路线 (共 743 条)
参考文献
Klason
Journal fuer Praktische Chemie (Leipzig), vol. <2> 33, p. 285
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Claus
Justus Liebigs Annalen der Chemie, vol. 179, p. 118
Chemische Berichte, vol. 9, p. 1915
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Laurent; Gerhardt
Annales de Chimie (Cachan, France), vol. <3> 19, p. 96
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Liebig
Justus Liebigs Annalen der Chemie, vol. 10, p. 10
反应条件
zeolite molecular sieve 4 Å in acetonitrile
1 h; Reflux;
参考文献
Eisavi, Ronak; Zeynizadeh, Behzad; Baradarani, Mohammad Mehdi
Bulletin of the Korean Chemical Society, 2011 , vol. 32, # 2 p. 630 - 634
反应条件
zeolite molecular sieve 4 Å in methanol
0.666667 h; Reflux;
参考文献
Eisavi, Ronak; Zeynizadeh, Behzad; Baradarani, Mohammad Mehdi
Bulletin of the Korean Chemical Society, 2011 , vol. 32, # 2 p. 630 - 634
反应条件
5,10,15,20-tetraphenyl-21H,23H-porphine Co(II) in acetonitrile
0.666667 h; Heating; Product distribution; Further Variations:CatalystsSolvents;
参考文献
Sharghi, Hashem; Nejad, Alireza Hassani; Nasseri, Mohammad Ali
New Journal of Chemistry, 2004 , vol. 28, # 8 p. 946 - 951
反应条件
bromine; triphenylphosphine in acetonitrile
T=20°C; Thiocyanation;
参考文献
Iranpoor; Firouzabadi; Shaterian
Journal of Chemical Research - Part S, 1999 , # 11 p. 676 - 677
反应条件
1: ammonium thiocyanate With PPh3.Br2 in acetonitrile
T=20°C;
2: 2-tetrahydropyranyl ether of 2-octanol in acetonitrile
T=20°C; Title compound not separated from byproducts;
参考文献
Iranpoor, Nasser; Firouzabadi, Habib; Shaterian, Hamid Reza
Phosphorus, Sulfur and Silicon and the Related Elements, 2005 , vol. 180, # 9 p. 2093 - 2096
反应条件
1: ammonium thiocyanate With APDPP; bromine in acetonitrile
T=20°C; 2 h;
2: trimethyl(1-methylheptyloxy)silane in acetonitrile
T=20°C; 0.0833333 h;
参考文献
Iranpoor, Nasser; Firouzabadi, Habib; Gholinejad, Mohammad
Phosphorus, Sulfur and Silicon and the Related Elements, 2009 , vol. 184, # 8 p. 2010 - 2019
反应条件
1: ammonium thiocyanate With APDPP; bromine in acetonitrile
T=20°C; 2 h;
2: 1-methylheptanol; trimethyl(1-methylheptyloxy)silane in acetonitrile
T=20°C; 0.0833333 h;
参考文献
Iranpoor, Nasser; Firouzabadi, Habib; Gholinejad, Mohammad
Phosphorus, Sulfur and Silicon and the Related Elements, 2009 , vol. 184, # 8 p. 2010 - 2019
参考文献
Rybin, A. G.; Zil'berman, E. N.; Trachenko, V. I.; Krasnov, V. L.
J. Gen. Chem. USSR (Engl. Transl.), 1981 , vol. 51, # 11 p. 2571 - 2574,2217 - 2219
反应条件
ethanol
Electrolysis;
参考文献
Melnikow; Sskljarenko; Tscherkassowa
Zhurnal Obshchei Khimii, 1939 , vol. 9, p. 1819,1821
Chem. Zentralbl., 1940 , vol. 111, # I p. 1641