1147550-11-5合成路线 (共 743 条)
反应条件
1: ammonium thiocyanate; benzoyl chloride in acetone
0.25 h; Heating;
2: 4-chloro-aniline in acetone
0.5 h; Heating;
参考文献
Wang, Xicun; Wang, Fang; Quan, Zhengjun; Zhang, Zhang; Wang, Mangang
Synthetic Communications, 2006 , vol. 36, # 17 p. 2453 - 2460
反应条件
1.) acetone, reflux, 1 h, 2.) acetone, reflux; Yield given. Multistep reaction;
参考文献
Sawhney, S. N.; Dhindsa, G. S.; Singh, S. P.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 10 p. 1044 - 1049
参考文献
Kaye; Parris
Journal of the American Chemical Society, 1952 , vol. 74, p. 2271
反应条件
1: ammonium thiocyanate; benzoyl chloride in acetone
0.25 h; Heating;
2: o-toluidine in acetone
0.5 h; Heating;
参考文献
Holla, B. Shivarama; Malini; Rao, B. Sooryanarayana; Sarojini; Kumari, N. Suchetha
European Journal of Medicinal Chemistry, 2003 , vol. 38, # 3 p. 313 - 318
反应条件
1.) Me2CO, 40 deg C, 30 min, 2.) Me2CO, 20 deg C, 2 h; Yield given. Multistep reaction;
参考文献
Brindley, Jocelyn C.; Caldwell, Jennifer M.; Meakins, G. Denis; Plackett, Simon J.; Price, Susan J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 1153 - 1158
反应条件
1: With benzoyl chloride in acetone
1 h; Heating;
2: With sodium hydroxide in water
Heating;
参考文献
Narayana; Vijaya Raj; Ashalatha; Kumari, N. Suchetha; Sarojini
European Journal of Medicinal Chemistry, 2004 , vol. 39, # 10 p. 867 - 872
反应条件
T=180 - 190°C; 1.5 h;
参考文献
Demina, L. M.; Konshin, M. E.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1992 , vol. 28, # 10 p. 1179 - 1181
Khimiya Geterotsiklicheskikh Soedinenii, 1992 , # 10 p. 1384 - 1386
反应条件
aluminum oxide; methanesulfonic acid
T=20°C; 1.08333 h; neat (no solvent); regioselective reaction;
参考文献
Hosseini-Sarvari, Mona; Tavakolian, Mina
Journal of Chemical Research, 2008 , # 6 p. 318 - 321
反应条件
Cu(BF4)2 in water; acetone
T=-10 - -5°C; 2 h;
参考文献
Grishchuk; Klimnyuk; Baranovskii; Boichak; Gorbovoi
Pharmaceutical Chemistry Journal, 2001 , vol. 35, # 7 p. 373 - 374
反应条件
aluminum oxide; methanesulfonic acid
T=20°C; 0.5 h; neat (no solvent);
参考文献
Hosseini-Sarvari, Mona; Tavakolian, Mina
Journal of Chemical Research, 2008 , # 6 p. 318 - 321