N-(4-甲氧基苯基)-4-甲基苯磺酰胺合成路线 （共 18 条）
参考文献
Reverdin
Chemische Berichte, 1909 , vol. 42, p. 1526
Chem. Zentralbl., 1909 , vol. 80, # I p. 1810
参考文献
Reverdin; de Luc
Chemische Berichte, 1910 , vol. 43, p. 3462
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1910 , vol. 151, p. 985
反应条件
bis-[(trifluoroacetoxy)iodo]benzene in dichloromethane Oxidation;
参考文献
Tohma, Hirofumi; Watanabe, Hiroaki; Takizawa, Shinobu; Maegawa, Tomohiro; Kita, Yasuyuki
Heterocycles, 1999 , vol. 51, # 8 p. 1785 - 1788
反应条件
sulfuric acid
T=110°C;
参考文献
Halberkann
Chemische Berichte, 1921 , vol. 54, p. 1665 Anm.1
参考文献
Halberkann
Chemische Berichte, 1921 , vol. 54, p. 1665 Anm.1
反应条件
1: 74 percent / 10percent aq NaOH / CHCl3 / 2 h / Ambient temperature
2: 73 percent / conc. Hydrochloric acid / 34 h / Heating
View Scheme
参考文献
Kurbatov, Yu. V.; Solekhova, M. A.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1986 , vol. 22, # 7 p. 749 - 751
Khimiya Geterotsiklicheskikh Soedinenii, 1986 , vol. 22, # 7 p. 936 - 938
反应条件
1: 77 percent / methanol / Ambient temperature; anodic oxidation, graphite felt anode, platinum cathode, one compartment cell, tetraethylammonium perchlorate
2: 95 percent / neutral alumina column / ethyl acetate
View Scheme
参考文献
Coutts, Ian G. C.; Culbert, Nicholas J.; Edwards, Mark; Hadfield, John A.; Musto, Donald R.; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1829 - 1836
反应条件
nitric acid; acetic acid
T=10 - 20°C; man loest das Nitrierungprod. in Bzl.und versetzt mit Ligroin;die sich ausscheidet Nadeln(3.5-Dinitro-,und 3-Nitro-4-p-toluolsulfamino-anisol)krystallisiert aus Essigs. oder Alk. um,verseift durch Schwefels.und giesst in Wss.;
参考文献
Reverdin
Chemische Berichte, 1909 , vol. 42, p. 1526
Chem. Zentralbl., 1909 , vol. 80, # I p. 1810
