[(R)-(+)-2,2'-双(二苯基膦)-1,1'-联萘]二氯化钯合成路线 （共 5 条）
反应条件
in benzene T=20°C; 2 h;
参考文献
BRISTOL-MYERS SQUIBB COMPANY
Patent: WO2006/138373 A2, 2006 ;
Location in patent: Page/Page column 98 ;
WO 2006/138373 A2
参考文献
Veron, Anna C.; Felber, Michael; Blacque, Olivier; Spingler, Bernhard
Polyhedron, 2013 , vol. 52, p. 102 - 105
反应条件
in benzene under N2; a soln. of the ligand in benzene was added to a mixt. of the Pd-complex and benzene, stirred overnight; filtered, washed with benzene, dried under vac., dissolved in acetone, layered with hexane, stand at room temp.; elem. anal.;
参考文献
Ozawa, Fumiyuki; Kubo, Akihiko; Matsumoto, Yonetatsu; Hayashi, Tamio; Nishioka, Eriko; et al.
Organometallics, 1993 , vol. 12, p. 4188 - 4196
反应条件
in dichloromethane Schlenk techniques, under N2 or Ar; according to P. Gugger, S.O. Limmer,A.A. Watson, A.C. Willis, S.B. Wild, Inorg. Chem. 32 (1993) 5692; phosp hine ligand reacted with equimolar amt. of Pd complex;
参考文献
Journal of Molecular Catalysis A: Chemical, , vol. 261, # 1 p. 112 - 119
反应条件
in benzene Treating Pd-comp. in benzene with stoich. amt. of ligand (N2).;
参考文献
Graaf, Wim de; Boersma, Jaap; Koten, Gerard van; Elsevier, Cornelis J.
Journal of Organometallic Chemistry, 1989 , vol. 378, p. 115 - 124
