1: With sodium hydride in N,N-dimethyl-formamide T=20 - 100°C; 10 h; Inert atmosphere; 2: With hydrogenchloride; water in tetrahydrofuran; N,N-dimethyl-formamide 2 h; RefluxInert atmosphere;
参考文献
The Scripps Research Insitiute
Patent: US2012/59179 A1, 2012 ;
Location in patent: Page/Page column 18 ;