in water byproducts: CO2, H2O; High Pressure; heated in autoclave at 550°C for 12 h; cooled to room temp., washed (aq. HCl), separated by flotation, filtered, washed (alcohol), dried (vac., 4 h, 60°C); XRD;
in neat (no solvent) byproducts: N2; powders were placed in autoclave, at 550°C for 10 h; ppt. was collected and washed with water and EtOH, dried in vac. at 65°C for 5h; XRD;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 79, # 8 p. 1312 - 1313
iron(III) chloride; 1,2-diphenyl-2-hydroxyethanone in acetonitrile T=140°C; P=18751.5 Torr; other temp.; other pressure; varying amount of catalyst; Product distribution;
参考文献
Battais, A.; Boutevin, B.; Pietrasanta, Y.; Bertocchio, R.; Lantz, A.
Journal of Fluorine Chemistry, 1989 , vol. 42, p. 215 - 232
