in tetrahydrofuran; methanol
96 h; Inert atmosphereMolecular sieveReflux;
参考文献
Li, Jie; Lutz, Martin; Spek, Anthony L.; Van Klink, Gerard P.M.; Van Koten, Gerard; Klein Gebbink, Robertus J.M.
Journal of Organometallic Chemistry, 2010 , vol. 695, # 24 p. 2618 - 2628
Carre, Francis H.; Chuit, Claude; Corriu, Robert J. P.; Douglas, William E.; Guy, Daniel M. H.; Reye, Catherine
European Journal of Inorganic Chemistry, 2000 , # 4 p. 647 - 653
1: 85 percent / 1.9 M n-BuLi / diethyl ether; hexane / 1 h / -20 - 0 °C
2: 55 percent / diethyl ether / 21 h
View Scheme
参考文献
Carre, Francis H.; Chuit, Claude; Corriu, Robert J. P.; Douglas, William E.; Guy, Daniel M. H.; Reye, Catherine
European Journal of Inorganic Chemistry, 2000 , # 4 p. 647 - 653