1165952-91-9合成路线 (共 295 条)
反应条件
Rh4(CO)14; hydrogen in hexane T=19.85°C; Hydroformylation; reaction was studied by in-situ high-pressure IR spectroscopy; Product distribution;
参考文献
Liu, Guowei; Garland, Marc
Journal of Organometallic Chemistry, 2000 , vol. 608, # 1-2 p. 76 - 85
反应条件
1: With boron trifluoride diethyl etherate in dichloromethane; trifluoroacetic acid T=-80°C; 2 h; 2: T=20°C; 72 h;
参考文献
Maison, Wolfgang; Adiwidjaja, Gunadi
Tetrahedron Letters, 2002 , vol. 43, # 34 p. 5957 - 5960
反应条件
water; trifluoroacetic acid in N,N-dimethyl-formamide 60 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Dyatkin, Alexey B.; Hoekstra, William J.; Hlasta, Dennis J.; Andrade-Gordon, Patricia; De Garavilla, Lawrence; Demarest, Keith T.; Gunnet, Joseph W.; Hageman, William; Look, Richard; Maryanoff, Bruce E.
Bioorganic and Medicinal Chemistry Letters, 2002 , vol. 12, # 21 p. 3081 - 3084
反应条件
water; trifluoroacetic acid in N,N-dimethyl-formamide 60 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Bailey, Patrick D.; Wilson, Robert D.; Brown, George R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 5 p. 1337 - 1340
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene T=20°C; 24 h;
参考文献
Utsunomiya, Masaru; Kawatsura, Motoi; Hartwig, John F.
Angewandte Chemie - International Edition, 2003 , vol. 42, # 47 p. 5865 - 5868
反应条件
aluminum oxide; Ni(acac) T=200°C; 12 h; other dialkyl sulfoxides and 1,3-dienes; var. metal complexes and ligands; var. stoichiometry; Product distributionMechanism;
参考文献
Dzhemilev, U. M.; Kunakova, R. V.; Baibulatova, N. Z.; Tarasenko, A. E.; Mustafina, E. M.
Bull. Russ. Acad. Sci. Div. Chem. Sci. (Engl. Transl.), 1992 , vol. 41, # 1 p. 160 - 166,128 - 134
反应条件
1: HCl / -8 °C 2: cold aqueous NaHCO3 View Scheme
参考文献
Berlande
Bulletin de la Societe Chimique de France, 1942 , vol. <5> 9, p. 644,651, 652
反应条件
bis(1,5-cyclooctadiene)nickel (0); diethylaluminium chloride; triphenylphosphine in toluene T=50°C; 48 h; other ligands, var. P/Ni and Al/Ni ratios, var. reaction times; Product distribution;
参考文献
Cros, Philippe; Triantaphylides, Christian; Buono, Gerard
Journal of Organic Chemistry, 1988 , vol. 53, # 1 p. 185 - 187
反应条件
copper acetylacetonate in acetonitrile T=-10 - 20°C;
参考文献
Tetrahedron Letters, , vol. 46, # 15 p. 2539 - 2542
反应条件
pyridine; pyridine 1-oxide; rac-nitridomanganese in dichloromethane T=0°C; Tosylation; aziridination; 0.5 h;
参考文献
Tetrahedron Letters, , vol. 41, # 36 p. 7089 - 7092