1165952-91-9合成路线 (共 295 条)
参考文献
Hofmann; Damm
Mitt. Kohlenforschungsinst. Breslau, vol. 2, p. 126
Chem. Zentralbl., 1926 , vol. 97, # I p. 2343
反应条件
triethylamine in ethanol 1 h; Irradiation;
参考文献
Pandey, Bipin; Dalvi, Pramod V.
Angewandte Chemie, 1993 , vol. 105, # 11 p. 1724 - 1726
反应条件
1: 2.) H2O / 1.) ether, RT, 1.5 h, 2.) RT, overnight 2: 81 mg / 0.17 h / 250 - 280 °C / other substituted bicyclo<2.2.2>oct-5-ene-trans-2,3-dicarboxylic acids and bicyclo<3.2.2>non-5-ene-trans-2,3-dicarboxylic acids View Scheme
参考文献
Weisz, Adrian; Mandelbaum, Asher
Journal of Organic Chemistry, 1988 , vol. 53, # 25 p. 5812 - 5815
反应条件
1: 75 percent / 168 h / Ambient temperature 2: SOCl2 / 2 h / Heating View Scheme
参考文献
Donkor, Isaac O.; Abdel-Ghany, Yasar S.; Kador, Peter F.; Mizoguchi, Tadashi; Bartoszko-Malik, Anita; Miller, Duane D.
European Journal of Medicinal Chemistry, 1999 , vol. 34, # 3 p. 235 - 243
反应条件
1: 48 h / 100 °C 2: 1.) NBS, benzoyl peroxide; 2.) aq. NaOH / 1.) CCl4, reflux, hν, 2 h; 2.) 20 deg C, 1 h View Scheme
参考文献
Harland, Philip A.; Hodge, Philip
Synthesis, 1983 , # 5 p. 419 - 421
反应条件
1: 80 percent / NaOH, chlorine chloride / Heating 2: 45 percent / Li / tetrahydrofuran / 0 - 5 °C View Scheme
参考文献
Grignon-Dubois, M.; Dunogues, J.; Ahra, M.
Recueil des Travaux Chimiques des Pays-Bas, 1988 , vol. 107, # 3 p. 216 - 225
反应条件
lithium 2.) THF; Multistep reaction;
参考文献
Grelier-Marly, Marie-Catherine; Grignon-Dubois, Micheline
Canadian Journal of Chemistry, 1994 , vol. 72, # 6 p. 1541 - 1547
反应条件
tetrakis(triphenylphosphine) palladium(0) in benzene T=20°C; 1 h; Inert atmosphere;
参考文献
Organic Letters, , vol. 15, # 7 p. 1728 - 1731
反应条件
in benzene (N2); added an excess of 1,3-cyclohexadiene to soln. of Ru-complex; refluxed for 5-10 min; evapd. (vac.); chromy.;;
参考文献
Organometallics, , vol. 10, p. 1260 - 1268
反应条件
in not given byproducts: cyclohexene, 1,4-cyclohexadiene; closed vessel; according to Giordano and Sappa, J. Organometal. Chem., 448 (1993) 157; TLC (SiO2, Et2O/light petroleum), gas chromy. of org. products;
参考文献
Castiglioni, Mario; Giordano, Roberto; Sappa, Enrico
Journal of Organometallic Chemistry, 1995 , vol. 491, # 1-2 p. 111 - 120