1165952-91-9合成路线 （共 295 条）
反应条件
bis(cyclopentadienyl)titanium dichloride; isopropylmagnesium chloride
1) THF, -20 deg C; 2.) THF, -20 deg C; Yield given. Multistep reaction;
参考文献
Szymoniak, Jan; Felix, Didier; Moise, Claude
Tetrahedron Letters, 1996 , vol. 37, # 1 p. 33 - 36
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; trifluoroacetic acid; bis(1,5-cyclooctadiene)nickel (0) in toluene
T=20°C; 20 h;
参考文献
Pawlas, Jan; Nakao, Yoshiaki; Kawatsura, Motoi; Hartwig, John F.
Journal of the American Chemical Society, 2002 , vol. 124, # 14 p. 3669 - 3679
反应条件
1: cyclohexa-1,3-diene With isopropylmagnesium chloride; [NiCl2Py4] in tetrahydrofuran
T=20°C; Addition; Hydromagnesation; 40 h;
2: carbon dioxide in tetrahydrofuran
Carboxylation;
参考文献
Viktorov; Zubritskii
Russian Journal of Organic Chemistry, 1999 , vol. 35, # 12 p. 1755 - 1765
反应条件
[2-(MeSO2NH)-2-phenylethyl]PPh2 palladium in dichloromethane
T=0°C; 40 h;
参考文献
Gustafsson; Bergqvist; Frejd
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 12 p. 1452 - 1457
反应条件
2: nickel; ethanol / Hydrogenation
3: ethanolic KOH
View Scheme
参考文献
Lewina; Godowikow
Zhurnal Obshchei Khimii, 1955 , vol. 25, p. 986,988; engl. Ausg. S. 951
反应条件
1: HCl / -8 °C
2: ethanol
View Scheme
参考文献
Berlande
Bulletin de la Societe Chimique de France, 1942 , vol. <5> 9, p. 644,651, 652
反应条件
hydroquinone; benzene
参考文献
Wildman; Saunders
Journal of Organic Chemistry, 1954 , vol. 19, p. 381,383
反应条件
hydroquinone in benzene
T=123 - 125°C; 17 h; Yield given. Yields of byproduct given;
参考文献
Carr, Richard V. C.; Williams, Richard V.; Paquette, Leo A.
Journal of Organic Chemistry, 1983 , vol. 48, # 25 p. 4976 - 4986
反应条件
bismuth trifluoromethanesulphonate; [Cu(I)(CH3CN)4]PF6; 1,2-bis-(diphenylphosphino)ethane in 1,4-dioxane
T=25°C; 24 h;
参考文献
Qin, Hongbo; Yamagiwa, Noriyuki; Matsunaga, Shigeki; Shibasaki, Masakatsu
Journal of the American Chemical Society, 2006 , vol. 128, # 5 p. 1611 - 1614
参考文献
Manolagas, Stavros C.; Katzenellenbogen, John A.
Patent: US2003/119800 A1, 2003 ;
