反应条件
1: 1.) LDA / 1.) THF, hexane, 23 deg C, 1 h, 2.) 23 deg C, 16 h 2: thionyl chloride / CH2Cl2 / 16 h / 23 °C 3: AlCl3 / CH2Cl2 / 0.5 h / 0 °C 4: 1.) L-Selectride, 2.) 10percent NaOH, 30percent H2O2 / 1.) THF, -78 deg C, 0.5 h, 2.) 0 deg C, 16 h View Scheme
参考文献
Halterman, Ronald L.; McEvoy, Marjorie A.
Journal of the American Chemical Society, 1990 , vol. 112, # 18 p. 6690 - 6695
