邻苯二甲酸二(2-乙基己基)酯合成路线 （共 11 条）
反应条件
titanium tetra-n-butoxide 100 h; further catalysts; mechanism of catalysis of the esterification; Mechanism;
参考文献
Doklady Chemistry, , vol. 295, # 8 p. 357 - 359
Dokl. Akad. Nauk SSSR Ser. Khim., , vol. 295, # 5 p. 1128 - 1130
反应条件
titanium tetra-n-butoxide 5.41667 h; azeotropic distillation;
参考文献
Oxeno Olefinchemie GmbH
Patent: EP1186593 A2, 2002 ;
Location in patent: Page 6 ;
反应条件
1: phthalic anhydride; 2-methyl-propan-1-ol T=130°C; 1 h; 2: 2-ethyl-n-hexanol; 2-methyl-propan-1-ol With tin oxide T=220°C; P=150.015 Torr; 7 h; Dean-Stark trap; Product distribution / selectivity;
参考文献
US2005/38283 A1, ;
Page/Page column 43 ;
反应条件
oxygen; ozone in water
参考文献
US2008/242875 A1, ;
Page/Page column 9-11; 17-18 ;
反应条件
potassium hydroxide; Aliquatreg; 336 1.) 60 deg C, 0.1 Torr, 6 h, 2.) 85 deg C, 24 h; Yield given. Multistep reaction;
参考文献
Synthesis, , # 1 p. 40 - 45
反应条件
sulfuric acid Heating; Title compound not separated from byproducts;
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 49, # 1 p. 253 - 266
反应条件
toluene-4-sulfonic acid
参考文献
Kogyo Kagaku Zasshi, , vol. 59, p. 895,897
Technology Reports of the Osaka University, , vol. 7, p. 199,203
反应条件
titanium tetra-n-butoxide 2.5 h; Heatingother catalysts other reaction time degree of esterification estimated by titration with KOH; Title compound not separated from byproducts;
参考文献
Novrocik, Jan; Novrocikova, Marta; Norek, Jiri; Koruna, Ivan; Ryska, Miroslav
Collection of Czechoslovak Chemical Communications, 1984 , vol. 49, # 1 p. 253 - 266
反应条件
Tris-HCl buffer; mouse hepatic microsomal esterase ES46.5K in acetone T=37°C; Hydrolysis; pH=8.0; Enzyme kinetics; Further Variations:Reagents;
参考文献
Biological and Pharmaceutical Bulletin, , vol. 20, # 7 p. 749 - 751
反应条件
hydrogen in hexane
T=159.84°C; P=30003 Torr;
参考文献
Zhao, Jie; Xue, Mingwei; Huang, Yuan; Shen, Jianyi
Catalysis Communications, 2011 , vol. 16, # 1 p. 30 - 34
