1: 80 percent / K2CO3, Cu / 3 h / 200 °C 2: 94 percent / K2CO3 / dimethylformamide / 12 h / Ambient temperature 3: 83 percent / LiAlH4 / tetrahydrofuran / 1 h / 0 °C 4: 50 percent / CrO3, pyridine / CH2Cl2 / 1 h / Ambient temperature View Scheme
参考文献
Calestani, Gianluca; Leardini, Rino; McNab, Hamish; Nanni, Daniele; Zanardi, Giuseppe
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 11 p. 1813 - 1824
1.1: thionyl chloride / Reflux 2.1: dichloromethane / 3 h / 0 - 20 °C 3.1: copper(l) iodide; 1,10-phenanthroline; water / 0.17 h / 20 °C 3.2: 10 h / 100 °C View Scheme
参考文献
Balkrishna, Shah Jaimin; Kumar, Sangit
Synthesis, 2012 , vol. 44, # 9 p. 1417 - 1426
1: ortho-chlorobenzoic acid With 1,1'-carbonyldiimidazole in tetrahydrofuran T=20°C; 0.166667 h; 2: 2-amino-phenol in tetrahydrofuran Heating; Further stages.;
参考文献
Kumar, Anil; Narasimhan, Balasubramanian; Kumar, Devinder
Bioorganic and Medicinal Chemistry, 2007 , vol. 15, # 12 p. 4113 - 4124
1: 2-mercapto benzoic acid With sodium hydride in N,N-dimethyl-formamide T=20°C; 2: ortho-chlorobenzoic acid With copper(I) oxide 5 h; RefluxInert atmosphere; Reagent/catalystSolventTimeTemperature;
参考文献
Moosun, Salma; Bhowon, Minu G.; Jhaumeer-Laulloo, Sabina; Joule, John A.
Phosphorus, Sulfur and Silicon and the Related Elements, 2012 , vol. 187, # 11 p. 1383 - 1400,18
