反应条件
1.1: sulfuric acid; copper; copper(II) sulfate; potassium bromide / water / 2 h / Reflux 1.2: 80 - 90 °C 2.1: thionyl chloride / diethyl ether / 2 h / Reflux 3.1: iron (III) acetylacetonate / diethyl ether / -78 °C / Inert atmosphere 4.1: Candida tenuis AKR2B5 xylose reductase [E.(1)C11175]; water; Reduced nicotinamide-adenine dinucleotide / ethanol / 25 °C / pH 7 / aq. phosphate buffer; Enzymatic reaction View Scheme
参考文献
Vogl, Michael; Kratzer, Regina; Nidetzky, Bernd; Brecker, Lothar
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 16 p. 5863 - 5870
