1-(乙氧基-乙硫基磷酰)氧基乙烷合成路线 （共 41 条）
反应条件
thiamine diphosphate; diethylazodicarboxylate in benzene T=35 - 40°C; 6 h; Yield given;
参考文献
Mlotkowska, B.; Wartalowska-Graczyk, M.
Journal fuer Praktische Chemie (Leipzig), 1987 , vol. 329, # 4 p. 735 - 740
反应条件
in diethyl ether T=20°C; 1.5 h;
参考文献
Abbott, Amberashley; Sierakowski, Tim; Kiddle, James J.; Clark, Kristin K.; Mezyk, Stephen P.
Journal of Physical Chemistry B, 2010 , vol. 114, # 22 p. 7681 - 7685
反应条件
dicyclohexyl-carbodiimide in diethyl ether 240 h; Ambient temperature;
参考文献
Mikolajczyk, Marian; Kielbasinski, Piotr; Basinski, Wlodzimierz
Journal of Organic Chemistry, 1984 , vol. 49, # 5 p. 899 - 908
反应条件
tetraphosphorus decasulfide in benzene T=78 - 96°C; 4.5 h; Yields of byproduct given;
参考文献
Mazitova, F. N.; Khairullin, V. K.
J. Gen. Chem. USSR (Engl. Transl.), 1980 , vol. 50, # 8 p. 1718 - 1722,1393 - 1396
反应条件
NOBF4 in water 15-30 min; Further byproducts given. Yields of byproduct given;
参考文献
Blankespoor, Ronald L.; Doyle, Michael P.; Smith, Daniel J.; Dyke, David A. Van; Waldyke, Michael J.
Journal of Organic Chemistry, 1983 , vol. 48, # 8 p. 1176 - 1179
参考文献
Kamalov, R. M.; Stepanov, G. S.; Pudovik, M. A.; Pudovik, A. N.
J. Gen. Chem. USSR (Engl. Transl.), 1990 , vol. 60, # 2.2 p. 476 - 477,414 - 415
参考文献
Kamalov, R. M.; Stepanov, G. S.; Pudovik, M. A.; Pudovik, A. N.
J. Gen. Chem. USSR (Engl. Transl.), 1990 , vol. 60, # 2.2 p. 476 - 477,414 - 415
参考文献
Pistschimuka
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, 1912 , vol. 44, p. 1439,1442
Journal fuer Praktische Chemie (Leipzig), 1911 , vol. <2>84, p. 748
Chem. Zentralbl., 1913 , vol. 84, # I p. 1581
参考文献
Jacobson et al.
Journal of the American Chemical Society, 1955 , vol. 77, p. 6064
反应条件
bis(diethoxyphosphoryl) disulfide in dichloromethane 1.) -70 deg C -> room temperature, 2.) room temperature, 30 min; Title compound not separated from byproducts;
参考文献
Krawczyk, Ewa; Skowronska, Aleksandra; Michalski, Jan
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 1 p. 89 - 100
