二(二甲基氨基)甲氧基甲烷合成路线 （共 18 条）
反应条件
in diethyl ether Heating;
参考文献
Chemische Berichte, , vol. 98, p. 1078 - 1080
反应条件
in tetrahydrofuran T=21°C; Title compound not separated from byproducts.;
参考文献
Advanced Synthesis and Catalysis, , vol. 346, # 9-10 p. 1081 - 1086
参考文献
Chemische Berichte, , vol. 105, p. 1340 - 1344
反应条件
Ambient temperature;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 58, # 6 p. 1445 - 1447,1289 - 1290
反应条件
T=17.9°C; ΔG(excit.), ΔH(excit.), ΔS(excit.); KineticsThermodynamic dataMechanism;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 993 - 996
反应条件
T=90°C; 0.333333 h; NMR study of reaction of various NN-dialkylformamide dimethyl acetals with secondary amines; Product distribution;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 1669 - 1672
参考文献
Tokmakov, G. P.; Zemlyanova, T. G.; Grandberg, I. I.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1986 , vol. 22, # 12 p. 1345 - 1349
Khimiya Geterotsiklicheskikh Soedinenii, 1986 , vol. 22, # 12 p. 1662 - 1667
反应条件
1: 8 h; Heating / reflux; 2: With hydrazine in butan-1-ol 6 h; Heating / reflux;
参考文献
TAKEDA CHEMICAL INDUSTRIES, LTD.
Patent: WO2003/99793 A1, 2003 ;
Location in patent: Page 272 ;
反应条件
dibenzoyl peroxide in chlorobenzene T=100°C; 3 h;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 21, # 4 p. 817 - 820
Zhurnal Organicheskoi Khimii, , vol. 21, # 4 p. 899 - 902
参考文献
Takeuchi, Naoki; Okada, Naomi; Tobinaga, Seisho
Chemical & Pharmaceutical Bulletin, 1983 , vol. 31, # 12 p. 4355 - 4359
