in neat (no solvent)
heating to 200°C in an autoclave;;
参考文献
Ashby, E. C.
Journal of the American Chemical Society, 1959 , vol. 81, p. 4791 - 4795
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Gmelin Handbook: B: B-Verb.14, 3.8.1.2.3, page 100 - 104
Lane, C. F.
Aldrichimica Acta, 1973 , vol. 6, p. 51 - 58
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Murray, L. T.
Diss. Abstr., Diss. Purdue Univ. 1963, S. 1/218 1964 , vol. 24, p. 5003
lithium triethylborohydride in tetrahydrofuran
successive addn. of LiBEt3H, butan-1-ol and hex-1-ene in THF to BH3 in THF; products are detected by (11)B-NMR;
参考文献
Arase, Akira; Nunokawa, Yutaka; Masuda, Yuzuru; Hoshi, Masayuki
Journal of the Chemical Society, Chemical Communications, 1992 , # 1 p. 51 - 52
in neat (no solvent)
Ar-atmosphere; addn. of Me3SiH (3 equivs.) to mixt. of hexene (3 equivs.) and BCl3 under reflux (12°C), stirring at room temp. for 2 h; not sepd.; NMR spectroscopy;
参考文献
Soundararajan, Raman; Matteson, Donald S.
Organometallics, 1995 , vol. 14, p. 4157 - 4166
