1,2,3,4-四氢萘合成路线 (共 818 条)
反应条件
hydrogen in ethanol T=39.84°C; P=760.051 Torr; 5 h;
参考文献
Gong; He; Zhao; Liu; Cui
Synthetic Communications, 2012 , vol. 42, # 4 p. 574 - 581
反应条件
sodium; tert-butyl alcohol in tetrahydrofuran 15 h; Heating;
参考文献
Menzek, Abdullah; Altundas, Aliye; Gueltekin, Demet
Journal of Chemical Research - Part S, 2003 , # 11 p. 752 - 753
反应条件
isopropyl alcohol; nickel 18 h; Heatingvarious aromatic compounds and reaction times; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 50, # 3 p. 394 - 396
反应条件
CoCl2.6H2O; lithium in tetrahydrofuran T=25°C; Birch reaction; 2.5 h; Inert atmosphere; regioselective reaction;
参考文献
Nador, Fabiana; Moglie, Yanina; Vitale, Cristian; Yus, Miguel; Alonso, Francisco; Radivoy, Gabriel
Tetrahedron, 2010 , vol. 66, # 24 p. 4318 - 4325
反应条件
2C2H3O2(1-)*Pd(2+)*3Na(1+)*C18H12O9PS3(3-); hydrogen; glycerol T=100°C; P=2250.23 Torr; 2 h; Schlenk technique;
参考文献
Chahdoura, Faouzi; Pradel, Christian; Gomez, Montserrat
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 18 p. 3648 - 3660
反应条件
sodium hydroxide; dihydrogen peroxide; dichloro(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) in tetrahydrofuran To a soln. of haloalkene is added 9-BBN at 0°C, mixt. is stirred for 5 h at room temp., catalyst and aq. NaOH are added, after refluxing for 14 h, the unreacted borane is oxidized with H2O2 for 1h.; Isolated by chromy. over silica gel with hexane-ether, identified by IR,(1)H NMR, mass spectrometry, elem. anal.;
参考文献
Miyaura, Norio; Ishiyama, Tatsuo; Sasaki, Hirotomo; Ishikawa, Masako; Satoh, Makoto; Suzuki, Akira
Journal of the American Chemical Society, 1989 , vol. 111, # 1 p. 314 - 321
反应条件
hydrogen; 30percent Cat 100 (Mm1.1Ni4.22Co0.42Al0.15Mn0.15)- 70percent USY (1percent Pd) in N-dodecane T=200°C; P=3345.86 Torr; Product distribution / selectivity;
参考文献
US7387712 B2, ;
Page/Page column 20-22; 25 ;
反应条件
nickel in ethanol T=150°C; P=91200.1 - 114000 Torr;
参考文献
Rao, M. Vishnumurthi; Bhatt, M. Vivekananda
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. <B> 20, # 4 p. 344 - 345
反应条件
hydrogen; lithium aluminium tetrahydride; titanium(III) chloride in hexane T=200°C; P=67505.4 Torr; 15 h; Yields of byproduct given;
参考文献
Yalpani, Mohamed
Chemische Berichte, 1990 , vol. 123, # 5 p. 983 - 987
参考文献
Givaudan Corporation
Patent: US4634548 A1, 1987 ;