1,2,3,4-四氢萘合成路线 (共 818 条)
反应条件
multistep, reduction of polycyclic arenes with tetraalkyldiboranes; further oxidation agent; deuteriolysis with CD3CO2D; Product distribution;
参考文献
Chemische Berichte, , vol. 122, p. 677 - 686
反应条件
N-(quinolin-2-ylmethylidene)aniline; copper(II) bis(trifluoromethanesulfonate); phenylhydrazine in acetone T=30°C; 5 h; Inert atmosphereSchlenk technique; Reagent/catalystTimeSolvent;
参考文献
Zhang, Bo; Zhu, Shou-Fei; Zhou, Qi-Lin
Tetrahedron, 2013 , vol. 69, # 8 p. 2033 - 2037
反应条件
N-(quinolin-2-ylmethylidene)aniline; copper(II) bis(trifluoromethanesulfonate); phenylhydrazine in 1,2-dichloro-ethane T=30°C; 12 h; Inert atmosphereSchlenk technique; Reagent/catalystTimeSolvent;
参考文献
Zhang, Bo; Zhu, Shou-Fei; Zhou, Qi-Lin
Tetrahedron, 2013 , vol. 69, # 8 p. 2033 - 2037
反应条件
tetra-(n-butyl)ammonium iodide in water T=80°C; 10 h;
参考文献
Feng, Jie; Liang, Shuai; Chen, Shan-Yong; Zhang, Ji; Fu, Song-Sen; Yu, Xiao-Qi
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 7 p. 1287 - 1292
反应条件
P=36775.4 Torr; Hydrogenation;
参考文献
I.G. Farbenind.
Patent: US1918648 , 1928 ;
Full Text Show Details
I.G. Farbenind.
Patent: DE545195 , 1927 ;
参考文献
Yakugaku Zasshi, , vol. 67, p. 243
Chem.Abstr., , p. 9508
参考文献
Noller
Journal of the American Chemical Society, 1929 , vol. 51, p. 597
Organic Syntheses, 1932 , vol. 12, p. 86
反应条件
4-tButyl iodoxybenzene in chlorobenzene T=130 - 140°C; 6 h;
参考文献
Tetrahedron Letters, , vol. 26, # 40 p. 4955 - 4956
反应条件
acetic acid; Zinc chloride in (2S)-N-methyl-1-phenylpropan-2-amine hydrate; water
参考文献
Takiguchi, Takao; Tsuboyama, Akira; Mizutani, Hidemasa; Okada, Shinjiro; Miura, Seishi; Moriyama, Takashi; Igawa, Satoshi; Kamatani, Jun; Furugori, Manabu
Patent: US2002/64681 A1, 2002 ;
反应条件
benzyltrimethylammonium bromide dibromide; zinc(II) chloride in acetic acid 1 h; Ambient temperature;
参考文献
Kajigaeshi, Shoji; Kakinami, Takaaki; Moriwaki, Masayuki; Tanaka, Toshio; Fujisaki, Shizuo; Okamoto, Tsuyoshi
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 2 p. 439 - 443