1,2,3,4-四氢萘合成路线 （共 818 条）
反应条件
1-butylhydroxyperoxide; bis-(triphenylsilyl oxide)dioxochromium in dichloromethane 24 h; Ambient temperature;
参考文献
Catino, Arthur J.; Nichols, Jason M.; Choi, Hojae; Gottipamula, Sidhartha; Doyle, Michael P.
Organic Letters, 2005 , vol. 7, # 23 p. 5167 - 5170
反应条件
1: 60 percent / tert-butyl hydroperoxide; NaHCO3 / dirhodium(II) tetrakis(caprolactamate)-acetonitrile (1/2) / 1,2-dichloro-ethane; decane / 16 h / 20 °C 2: 27 percent / tert-butyl hydroperoxide; NaHCO3 / dirhodium(II) tetrakis(caprolactamate)-acetonitrile (1/2) / 1,2-dichloro-ethane; decane / 16 h / 20 °C View Scheme
参考文献
Hsu, Shih-Fan; Plietker, Bernd
ChemCatChem, 2013 , vol. 5, # 1 p. 126 - 129
反应条件
pyridine-2-carboxylic acid; [Mn(ClO4)2]*6H2O; dihydrogen peroxide; sodium acetate in acetonitrile T=0 - 20°C;
参考文献
Dong, Jia Jia; Unjaroen, Duenpen; Mecozzi, Francesco; Harvey, Emma C.; Saisaha, Pattama; Pijper, Dirk; De Boer, Johannes W.; Alsters, Paul; Feringa, Ben L.; Browne, Wesley R.
ChemSusChem, 2013 , vol. 6, # 9 p. 1774 - 1778
反应条件
oxygen T=120°C; 24 h; Catalytic behavior; SolventTimeReagent/catalyst; chemoselective reaction;
参考文献
Dhakshinamoorthy, Amarajothi; Primo, Ana; Concepcion, Patricia; Alvaro, Mercedes; Garcia, Hermenegildo
Chemistry - A European Journal, 2013 , vol. 19, # 23 p. 7547 - 7554
反应条件
T=190°C; P=15200 Torr; Hydrogenation;
参考文献
v. Braun; Gmelin; Schultheiss
Chemische Berichte, 1923 , vol. 56, p. 1343
反应条件
sulfuric acid; nitric acid
参考文献
Schroeter
Justus Liebigs Annalen der Chemie, 1922 , vol. 426, p. 132
反应条件
nitric acid; acetic anhydride T=20°C; 2 h;
参考文献
Fortin, Jessica S.; Cote, Marie-France; Lacroix, Jacques; Desjardins, Michel; Petitclerc, Eric; C.-Gaudreault, Rene
Bioorganic and Medicinal Chemistry, 2008 , vol. 16, # 15 p. 7277 - 7290
反应条件
1: 2-methyl-acryloyl chloride With AlCl3, aluminium chloride in dichloromethane T=-70°C; 0.333333 h; 2: 1,2,3,4-tetrahydro-naphthalene in dichloromethane T=-70 - 20°C; 16 h;
参考文献
BASELL POLYOLEFINE GMBH
Patent: WO2005/58916 A2, 2005 ;
Location in patent: Page/Page column 45 ;
反应条件
aluminium trichloride in dichloromethane 5 h; Ambient temperature;
参考文献
Foster, Patrick; Rausch, Marvin D.; Chien, James C.W.
Journal of Organometallic Chemistry, 1998 , vol. 571, # 2 p. 171 - 181
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; iodine; hexacarbonyl chromium 1.) dibutyl ether, THF, 24 h, reflux, 2.) THF, -78 deg C, 1 h, 3.) THF, 0 deg C, 4 h, 4.) THF, -78 deg C, 5.) THF, 16 h, room temp.; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Cambie, Richard C.; Clark, George R.; Gallagher, Stewart R.; Rutledge, Peter S.; Stone, Martin J.; Woodgate, Paul D.
Journal of Organometallic Chemistry, 1988 , vol. 342, p. 315 - 338
