1,2,3,4-四氢萘合成路线 （共 818 条）
反应条件
1: 92 percent / Br2 / CCl4 / 1.5 h / 0 °C / Irradiation 2: 95 percent / t-BuOK / tetrahydrofuran / 20 °C View Scheme
参考文献
Horner; Winkelmann
Angewandte Chemie, 1959 , vol. 71, p. 349,356
反应条件
bromine in perfluorohexane 0.666667 h; Irradiation;
参考文献
Windmon, Nicole; Dragojlovic, Veljko
Tetrahedron Letters, 2008 , vol. 49, # 46 p. 6543 - 6546
反应条件
hydrogen sulfide; hydrogen T=350°C; Gas phase;
参考文献
Nassreddine, Salim; Massin, Laurence; Aouine, Mimoun; Geantet, Christophe; Piccolo, Laurent
Journal of Catalysis, 2011 , vol. 278, # 2 p. 253 - 265
反应条件
1: AlCl3 / benzene 2: N2H4*H2O, KOH / bis-(2-hydroxy-ethyl) ether / Heating 3: H2SO4 4: Pd-C / Heating 5: (saponification) View Scheme
参考文献
Dillenschneider,J.-P.; Maire,J.-C.
Bulletin de la Societe Chimique de France, 1964 , p. 2606 - 2609
反应条件
1.1: AlCl3, aluminium chloride / tetrachloroethane, 1,1,2,2- / 20 °C / Cooling with ice 2.1: hydrazine hydrate / diethylene glycol / 0.5 h / 20 °C 2.2: 120 - 215 °C 3.1: sulfuric acid / Reflux 4.1: palladium 10 on activated carbon / triglyme (triethylene glycol dimethyl ether) / 4 h / 240 °C / Inert atmosphere 5.1: methanesulfonic acid / 0.5 h / 90 °C / Inert atmosphere 6.1: n-butyllithium; N-cyclohexyl-N-isopropylamine / tetrahydrofuran; hexane / -78 °C / Inert atmosphere 6.2: 1 h / -78 °C / Inert atmosphere 7.1: palladium 10 on activated carbon / triglyme (triethylene glycol dimethyl ether) / 4 h / 240 °C / Inert atmosphere 8.1: diisobutylaluminium hydride / hexane; toluene / 1 h / -78 °C / Inert atmosphere 8.2: Inert atmosphere 9.1: methanesulfonic acid / dichloromethane / 0.5 h / 20 °C / Cooling with ice View Scheme
参考文献
Zhang, Zhenfa; Sangaiah, Ramiah; Gold, Avram; Ball, Louise M.
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 15 p. 5431 - 5435
参考文献
Fourneau; Billeter
Bulletin de la Societe Chimique de France, 1940 , vol. <5> 7, p. 593,597
反应条件
1: AlCl3 2: aluminium isopropylate 3: concentrated H2SO4 4: palladium/charcoal / 320 °C View Scheme
参考文献
Vig et al.
Journal of the Indian Chemical Society, 1955 , vol. 32, p. 697,700
反应条件
1: 92 percent / Br2 / CCl4 / 1.5 h / 0 °C / Irradiation 2: 95 percent / t-BuOK / tetrahydrofuran / 20 °C 3: 80 percent / dimethylformamide / 20 h / Heating View Scheme
参考文献
Cakmak, Osman; Kahveci, Ismail; Demirtas, Ibrahim; Hoekelek, Tuncer; Smith, Keith
Collection of Czechoslovak Chemical Communications, 2000 , vol. 65, # 11 p. 1791 - 1804
反应条件
in water T=25°C; 72 h; by Helminthosporium species; Yield given;
参考文献
Holland, Herbert L.; Bergen, Eleanor J.; Chenchaiah, P. Chinna; Khan, Shaheer H.; Munoz, Benito; et al.
Canadian Journal of Chemistry, 1987 , vol. 65, p. 502 - 507
反应条件
Pseudomonas monteilii TA-5 cells T=30°C; pH=7.0; 7 h; aq. phosphate bufferEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Lie, Felicia; Chen, Yongzheng; Wang, Zunsheng; Li, Zhi
Tetrahedron Asymmetry, 2009 , vol. 20, # 10 p. 1206 - 1211
