1,2,3,4-四氢萘合成路线 (共 818 条)
参考文献
Barbot
Bulletin de la Societe Chimique de France, 1930 , vol. <4> 47, p. 1314,1318
反应条件
acetophenone; 1,3,4,5,6,7,8-heptafluoro-2-naphthylhydrazine
24 h; Heating;
参考文献
Brooke, Gerald M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 821 - 826
反应条件
calcium shot; ethylenediamine; methylamine
24 h; Yields of byproduct given;
参考文献
Benkeser, Robert A.; Belmonte, Frank G.; Yang, Mei-Hui
Synthetic Communications, 1983 , vol. 13, # 13 p. 1103 - 1116
反应条件
white sand; calcium; tert-butyl alcohol in ethylenediamine
T=0°C; 24 h; Yield given. Yields of byproduct given;
参考文献
Benkeser, Robert A.; Laugal, James A.; Rappa, Angela
Tetrahedron Letters, 1984 , vol. 25, # 20 p. 2089 - 2092
反应条件
ammonia; sodium in methanol
T=-75 - -33°C; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Beger, J.; Thomas, B.; Vogel, T.; Kirmse, K.; Lang, R.
Journal fuer Praktische Chemie (Leipzig), 1991 , vol. 333, # 3 p. 481 - 488
反应条件
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
House, Herbert O.; Lee, Joseph H. C.; VanDerveer, Don; Wissinger, Jane E.
Journal of Organic Chemistry, 1983 , vol. 48, # 26 p. 5285 - 5288
反应条件
hydrogen; shungite carbon
T=285 - 320°C; Decomposition; rearrangement, dehydrogenation; P=37503 Torr; 6 h; KineticsProduct distribution; Further Variations:Catalysts;
参考文献
Grigor'eva; Rozhkova
Russian Journal of Applied Chemistry, 2000 , vol. 73, # 4 p. 639 - 644
反应条件
1: aluminium chloride / 50 - 70 °C
2: aluminium chloride / 70 - 80 °C
3: sulfur / 220 °C
View Scheme
参考文献
Zhang, Zhenfa; Sangaiah, Ramiah; Gold, Avram; Ball, Louise M.
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 15 p. 5431 - 5435
反应条件
T=150 - 200°C; P=15200 Torr; Hydrogenation;
参考文献
Schroeter, Tetralin-Ges.
Patent: DE352719 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 14, p. 834
Full Text Show Details
Schroeter; Mueller; Huang
Chemische Berichte, 1929 , vol. 62, p. 649
Full Text Show Details
Schroeter
Chemische Berichte, 1924 , vol. 57, p. 2014
Chem. Zentralbl., 1928 , vol. 99, # II p. 1386
反应条件
1: sulfuric acid; nitric acid / <40
2: nitric acid
View Scheme
参考文献
Schroeter
Justus Liebigs Annalen der Chemie, 1922 , vol. 426, p. 132