1,2,3,4-四氢萘合成路线 (共 818 条)
参考文献
Krollpfeiffer; Schaefer
Chemische Berichte, 1923 , vol. 56, p. 630
反应条件
1: AlCl3, EtNO2
2: H+, molecular sieves
3: H2 / Pd/C / acetic acid
View Scheme
参考文献
Dillenschneider,J.-P.; Maire,J.-C.
Bulletin de la Societe Chimique de France, 1964 , p. 2606 - 2609
反应条件
T=207°C; 96 h; Product distributionMechanism;
参考文献
Meier, Herbert; Konnerth, Ursula; Graw, Sylvia; Echter, Toni
Chemische Berichte, 1984 , vol. 117, # 1 p. 107 - 126
反应条件
1: aluminium chloride / 50 - 70 °C
2: aluminium chloride / 70 - 80 °C
3: phosphorus pentoxide / 175 °C
4: alkali; sodium hypochlorite
View Scheme
参考文献
Schroeter
Chemische Berichte, 1924 , vol. 57, p. 2014
Chem. Zentralbl., 1928 , vol. 99, # II p. 1386
反应条件
hydrogenchloride
Einleiten von HCl;
参考文献
Badger; Cook; Crosbie
Journal of the Chemical Society, 1947 , p. 1432
Full Text Show Details
I.G. Farbenind.
Patent: DE533850 , 1929 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 18, p. 585
Full Text Show Details
Gen. Aniline Works
Patent: FR695095 , 1930 ;
Full Text Show Details
Gen. Aniline Works
Patent: US1910462 , 1930 ;
反应条件
Multistep reaction. Title compound not separated from byproducts;
参考文献
Kido, Yoshiyuki; Yoshimura, Satoru; Yamaguchi, Masahiko; Uchimaru, Tadafumi
Bulletin of the Chemical Society of Japan, 1999 , vol. 72, # 7 p. 1445 - 1458
反应条件
anthracene; antimony trichloride
T=80°C; 0.5 h;
参考文献
Buchanan, A. C.; Dworkin, A. S.; Smith, G. P.
Journal of Organic Chemistry, 1982 , vol. 47, # 4 p. 603 - 607
反应条件
antimony trichloride
T=80°C; 0.5 h; var. polycyclic aromatic hydrocarbons; var. tetralin/anthracene ratios; Product distributionMechanism;
参考文献
Buchanan, A. C.; Dworkin, A. S.; Smith, G. P.
Journal of Organic Chemistry, 1982 , vol. 47, # 4 p. 603 - 607
参考文献
Orlow; Lichatschew
Chemische Berichte, 1930 , vol. 63, p. 2179,2183
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, 1930 , vol. 62, p. 1907,1910, 1912
反应条件
1: AlCl3, EtNO2
2: H+, molecular sieves
4: diethyl ether
5: TosOH / benzene / Heating
6: Pd/C / Heating
View Scheme
参考文献
Chirico, R. D.; Hossenlopp, I. A.; Nguyen, A.; Steele, W. V.; Gammon, B. E.
Journal of Chemical Thermodynamics, 1989 , vol. 21, # 2 p. 179 - 202