1,2,3,4-四氢萘合成路线 （共 818 条）
参考文献
Schroeter
Chemische Berichte, 1924 , vol. 57, p. 2014
Chem. Zentralbl., 1928 , vol. 99, # II p. 1386
反应条件
1: chlorosulfonic acid / -10 - -5 °C / und Kochen des entstandenen Chloridgemisches mit Wasser
2: durch Kalischmelze
3: potassium carbonate / 160 - 170 °C / 7600 Torr
4: hydrochloric acid
View Scheme
参考文献
Schroeter
Justus Liebigs Annalen der Chemie, 1922 , vol. 426, p. 132
反应条件
styrene-4-vinyl(N-alkylpyridinium bromide) in water; acetic acid
T=23°C; 24 h;
参考文献
Zajc, Barbara; Zupan, Marko
Tetrahedron, 1989 , vol. 45, # 24 p. 7869 - 7878
反应条件
aluminium trichloride
T=50 - 70°C;
参考文献
Barbot
Bulletin de la Societe Chimique de France, 1930 , vol. <4> 47, p. 1314,1318
反应条件
aluminium trichloride
T=50 - 70°C; 7 h; Further byproducts given;
参考文献
Wilson, Michael A.; Rottendorf, Horst; Collin, Philip J.; Vasallo, Anthony M.
Australian Journal of Chemistry, 1984 , vol. 37, # 11 p. 2379 - 2383
反应条件
iodine; silver nitrate in dichloromethane
T=0 - 20°C; 70 - 72 h; Product distribution / selectivity;
参考文献
ASTRAZENECA AB; ASTEX THERAPEUTICS LTD
Patent: WO2007/58602 A2, 2007 ;
Location in patent: Page/Page column 118; 208-209 ;
WO 2007/058602 A2
反应条件
T=205°C; P=11032.6 Torr; Hydrogenation;
参考文献
Cook
Journal of the Chemical Society, 1933 , p. 1592,1596
反应条件
1: AlCl3 / CCl4 / -5 - 0 °C
2: Al(OiPr)3 / propan-2-ol / Heating
View Scheme
参考文献
Casagrande,C.; Ferrari,G.
Farmaco, Edizione Scientifica, 1966 , vol. 21, p. 229 - 248
反应条件
1,1,8,8,22,22,29,29-octamethyl-1,8,22,29-tetraazonialt;8.1.8.1gt;paracyclophane tetrachloride; chlorine in water
Irradiationvar. of reagents; Product distribution;
参考文献
Schneider, Hans-Joerg; Philippi, Klaus
Chemische Berichte, 1984 , vol. 117, # 10 p. 3056 - 3074
反应条件
carbon disulfide; aluminium trichloride
参考文献
Bahner et al.
Journal of the American Chemical Society, 1951 , vol. 73, p. 4011
