1,2,3,4-四氢萘合成路线 （共 818 条）
反应条件
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
House, Herbert O.; Lee, Joseph H. C.; VanDerveer, Don; Wissinger, Jane E.
Journal of Organic Chemistry, 1983 , vol. 48, # 26 p. 5285 - 5288
反应条件
1: aluminium chloride / 50 - 70 °C
2: bei der Zinkstaubdestillation
3: nickel catalyst; tetralin / 120 - 150 °C / 7600 - 15200 Torr / Hydrogenation
4: nickel; tetralin / 180 °C / 10640 Torr / Hydrogenation
5: chloroform; bromine
View Scheme
参考文献
Schroeter
Chemische Berichte, 1924 , vol. 57, p. 2014
Chem. Zentralbl., 1928 , vol. 99, # II p. 1386
反应条件
1: aluminium chloride / 50 - 70 °C
2: Cr2O3-H2SO4
View Scheme
参考文献
Christol,H. et al.
Bulletin de la Societe Chimique de France, 1960 , p. 1576 - 1581
参考文献
Mentzer; Massicot
Bulletin de la Societe Chimique de France, 1956 , p. 144,146
反应条件
1: sodium; liquid NH3; ethanol
2: peroxybenzoic acid; chloroform
View Scheme
参考文献
Hueckel; Woerffel
Chemische Berichte, 1956 , vol. 89, p. 2098,2101
反应条件
bromine in tetrachloromethane
T=77°C; 0.166667 h; Further byproducts given;
参考文献
Cakmak, Osman; Kahveci, Ismail; Demirtas, Ibrahim; Hoekelek, Tuncer; Smith, Keith
Collection of Czechoslovak Chemical Communications, 2000 , vol. 65, # 11 p. 1791 - 1804
反应条件
1: bromine / |Inert atmosphere
2: acetone; water / |Inert atmosphere
View Scheme
参考文献
Draper, Richard W.; Hou, Donald
Organic Process Research and Development, 1998 , vol. 2, # 3 p. 175 - 185
反应条件
1: 1.) conc. HCl, conc. H2SO4, 2.) glacial AcOH, AcONa*3H2O, 3.) 4M NaOH, 4.) pyridinium dichromate, silica gel
2: 79 percent / sodium borohydride / ethanol / 1.5 h
View Scheme
参考文献
Horn Jensen, Eva; Nielsen, Per Halfdan
Heterocycles, 1995 , vol. 41, # 11 p. 2441 - 2458
反应条件
hydrogenchloride; sodium hydroxide; sulfuric acid; sodium acetate; acetic acid
Yield given. Multistep reaction. Title compound not separated from byproducts;
参考文献
Horn Jensen, Eva; Nielsen, Per Halfdan
Heterocycles, 1995 , vol. 41, # 11 p. 2441 - 2458
反应条件
aluminium trichloride in chlorobenzene
T=3 - 20°C; Formylation; 4.5 h;
参考文献
Kantlehner, Willi; Vettel, Markus; Gissel, Alexander; Haug, Erwin; Ziegler, Georg; Ciesielski, Michael; Scherr, Oliver; Haas, Richard
Advanced Synthesis and Catalysis, 2000 , vol. 342, # 3 p. 297 - 310
