119072-55-8合成路线 （共 225 条）
反应条件
1,3-bis-(diphenylphosphino)propane; caesium carbonate; palladium dichloride in toluene
16 h; Inert atmosphereReflux;
参考文献
Geden, Joanna V.; Pancholi, Alpa K.; Shipman, Michael
Journal of Organic Chemistry, 2013 , vol. 78, # 8 p. 4158 - 4164
反应条件
1,3-bis-(diphenylphosphino)propane; caesium carbonate; palladium dichloride in toluene
16 h; Inert atmosphereReflux;
参考文献
Geden, Joanna V.; Pancholi, Alpa K.; Shipman, Michael
Journal of Organic Chemistry, 2013 , vol. 78, # 8 p. 4158 - 4164
参考文献
Yamamoto,Y. et al.
Bulletin of the Chemical Society of Japan, 1975 , vol. 48, p. 3682 - 3685
Full Text Show Details
Yamamoto,Y. et al.
Tetrahedron Letters, 1974 , p. 793 - 796
反应条件
in tetrahydrofuran
T=20°C; 9 h;
参考文献
Ripka, Amy S.; Diaz, David D.; Sharpless, K. Barry; Finn
Organic Letters, 2003 , vol. 5, # 9 p. 1531 - 1533
反应条件
Yield given. Multistep reaction;
参考文献
Maeda, Hajime; Matsuya, Takahiro; Kambe, Nobuaki; Sonoda, Noboru; Fujiwara, Shin-Ichi; Shin-Ike, Tsutomu
Tetrahedron, 1997 , vol. 53, # 36 p. 12159 - 12166
反应条件
1: BF3-Et2O / CH2Cl2
2: aq. HCl
View Scheme
参考文献
Saegusa,T. et al.
Journal of Organic Chemistry, 1969 , vol. 34, # 12 p. 4040 - 4046
反应条件
water; triphenylphosphine; cesium fluoride; palladium dichloride in dimethyl sulfoxide
T=90°C;
参考文献
Jiang, Huanfeng; Liu, Bifu; Li, Yibiao; Wang, Azhong; Huang, Huawen
Organic Letters, 2011 , vol. 13, # 5 p. 1028 - 1031
反应条件
potassium fluoride; 18-crown-6 ether; water in tetrahydrofuran
T=30°C; 16 h; Inert atmosphere;
参考文献
Kaicharla, Trinadh; Thangaraj, Manikandan; Biju, Akkattu T.
Organic Letters, 2014 , vol. 16, # 6 p. 1728 - 1731
反应条件
potassium fluoride; 18-crown-6 ether; water in tetrahydrofuran
T=30°C; 16 h; Inert atmosphere; Overall yield = 79 percent; Overall yield = 0.09 g; regioselective reaction;
参考文献
Kaicharla, Trinadh; Thangaraj, Manikandan; Biju, Akkattu T.
Organic Letters, 2014 , vol. 16, # 6 p. 1728 - 1731
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; caesium carbonate; palladium dichloride in toluene
2 h; RefluxInert atmosphere;
参考文献
Bochatay, Valentin N.; Boissarie, Patrick J.; Murphy, John A.; Suckling, Colin J.; Lang, Stuart
Journal of Organic Chemistry, 2013 , vol. 78, # 4 p. 1471 - 1477
