119072-55-8合成路线 （共 225 条）
反应条件
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Buchwald, Stephen L.; LaMaire, Susan J.
Tetrahedron Letters, 1987 , vol. 28, # 3 p. 295 - 298
反应条件
in dichloromethane; water
参考文献
ACS Combinatorial Science, , vol. 13, # 1 p. 89 - 95
反应条件
water; tetraundecylcalix[4]recorcinolarene in chloroform-d1 T=60°C; 18 h; Catalytic behavior; Concentration;
参考文献
Bianchini, Giulio; Sorella, Giorgio La; Canever, Nicolo; Scarso, Alessandro; Strukul, Giorgio
Chemical Communications, 2013 , vol. 49, # 46 p. 5322 - 5324
反应条件
1: 85 percent / ZnCl2 / tetrahydrofuran; diethyl ether / 72 h / -25 °C 2: 1.) HCl / 1.) MeOH, 2.) H2O 3: 1.) 6N HCl, 2.) Amberlite IR-120 / 1.) 80 deg C View Scheme
参考文献
Kunz, Horst; Pfrengle, Waldemar; Sager, Wilfried
Tetrahedron Letters, 1989 , vol. 30, # 31 p. 4109 - 4110
反应条件
zinc(II) chloride in dichloromethane T=23°C; 12 h;
参考文献
Abu-El-Halawa, Rajab; Jochims, Johannes C.
Chemische Berichte, 1983 , vol. 116, # 5 p. 1834 - 1847
反应条件
dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct; caesium carbonate in toluene 16 h; Inert atmosphereReflux;
参考文献
Geden, Joanna V.; Pancholi, Alpa K.; Shipman, Michael
Journal of Organic Chemistry, 2013 , vol. 78, # 8 p. 4158 - 4164
反应条件
sulfur; Mo(O)(S2CNEt2)2 in acetone T=56°C; 72 h;
参考文献
Adam, Waldemar; Bargon, Rainer M.; Bosio, Sara G.; Schenk, Wolfdieter A.; Stalke, Dietmar
Journal of Organic Chemistry, 2002 , vol. 67, # 20 p. 7037 - 7041
反应条件
in various solvent(s) T=0°C; 1 h; Further byproducts given;
参考文献
Minozzi, Matteo; Nanni, Daniele; Walton, John C.
Journal of Organic Chemistry, 2004 , vol. 69, # 6 p. 2056 - 2069
反应条件
sodium tris(acetoxy)borohydride T=-40 - 0°C; 7 h;
参考文献
Kiselyov, Alexander S.
Tetrahedron Letters, 2005 , vol. 46, # 26 p. 4487 - 4490
反应条件
titanium tetrachloride in dichloromethane 1.) -50 deg C, 2.) 3 h room temperature;
参考文献
Tetrahedron Letters, , vol. 27, # 26 p. 2979 - 2980
