5-乙基-3,4-二氢-2H-吡咯合成路线 (共 16 条)
反应条件
in diethyl ether 1.) -20 deg C, 30 min, 2.) 25 deg C, 1h; or with EtMgBr;
参考文献
Hua, Duy H.; Miao, Shou Wu; Bharathi, S. Narasimha; Katsuhira, Takeshi; Bravo, Ana A.
Journal of Organic Chemistry, 1990 , vol. 55, # 11 p. 3682 - 3684
反应条件
n-butyllithium; diisopropylamine 1) THF, hexane, -78 deg C, 1 h; 2) THF, hexane, -78 deg C, 2 h, rt, 12 h; Yield givenMultistep reaction;
参考文献
Tehrani, Kourosch Abbaspour; Borremans, Didier; De Kimpe, Norbert
Tetrahedron, 1999 , vol. 55, # 13 p. 4133 - 4152
反应条件
sulfuric acid Bei der elektrolytischen Reduktion;
参考文献
Dennstedt
Patent: DE127086 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 6, p. 1215
反应条件
CaO Heating; Yield given;
参考文献
Ananthapadmanabhan, S.; Raja, T. K.; Srinivasan, V.; Simon, A.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1988 , vol. 27, p. 580
反应条件
1: With tert.-butylhydroperoxide; selenium(IV) oxide in dichloromethane T=20°C; 9 h; 2: With triphenylphosphine in dichloromethane T=0°C; 12 h;
参考文献
Fuganti, Claudio; Gatti, Francesco G.; Serra, Stefano
Tetrahedron, 2007 , vol. 63, # 22 p. 4762 - 4767
反应条件
platinum Hydrogenation;
参考文献
Craig; Bulbrook; Hixon
Journal of the American Chemical Society, 1931 , vol. 53, p. 1833