2,2,6,6-四甲基环己酮合成路线 （共 45 条）
反应条件
1.) from -100 deg C to RT.; Yield given. Multistep reaction;
参考文献
Hogeveen, H.; Menge, W. M. P. B.
Tetrahedron Letters, 1986 , vol. 27, # 24 p. 2767 - 2770
反应条件
water; 4,7,13,18-tetraoxa-1,10-diazabicyclo[8.5.5]eicosane in diethyl ether
Ambient temperature; Product distribution;
参考文献
Perraud, Robert; Handel, Henri; Pierre, Jean-Louis
Bulletin de la Societe Chimique de France, 1980 , vol. 2, # 5-6 p. 283 - 288
反应条件
T=609.9°C; Flash vacuum thermolysis (f.v.t.) at various temperatures (423, 631, 753, 783, 883, 1043 K).; Product distributionMechanism;
参考文献
Carlsen, Lars; Egsgaard, Helge; Schaumann, Ernst
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1980 , p. 1206 - 1211
参考文献
Laakso
Suomen Kemistilehti B, 1940 , vol. 13, p. 12
Chem.Abstr., 1940 , p. 5060
反应条件
Behandeln mit Methyljodid;
参考文献
Haller
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1913 , vol. 157, p. 180
反应条件
sodium tetrahydroborate in methanol; water
参考文献
Smith, John R. Lindsay; Thomas, C. Barry; Whittaker, Mark
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1993 , # 11 p. 2191 - 2194
反应条件
1: With tris[3,5-bis(2,2'',6,6''-tetramethyl-m-terphenyl-5'-yl)phenyl]phosphine; copper(l) chloride; sodium t-butanolate in toluene
T=20°C; 2 h; Inert atmosphere;
2: With hydrogenchloride; methanol in toluene
Inert atmosphere;
参考文献
Fujihara, Tetsuaki; Semba, Kazuhiko; Terao, Jun; Tsuji, Yasushi
Angewandte Chemie - International Edition, 2010 , vol. 49, # 8 p. 1472 - 1476
反应条件
hydroxylamine hydrochloride; sodium acetate in methanol
72 h; Heating;
参考文献
Filip, Sorin V.; Sewald, Norbert
Synthesis, 2005 , # 20 art. no. T06205SS, p. 3565 - 3570
反应条件
in tetrahydrofuran
T=-76°C; 1 h;
参考文献
Collins, David J.; Jacobs, Howard A.
Australian Journal of Chemistry, 1987 , vol. 40, # 12 p. 1989 - 2004
反应条件
in pentane
T=0°C; 20 h; Irradiation;
参考文献
Hinsberg, William D.; Schultz, Peter G.; Dervan, Peter B.
Journal of the American Chemical Society, 1982 , vol. 104, # 3 p. 766 - 773
