1197040-29-1合成路线 （共 99 条）
反应条件
1: 2.) TMEDA / 1.) ether, -78 deg C, 15 min; 2.) below 0 deg C, then r.t., 6 h
2: 47 percent / diethyl ether / 48 h / Ambient temperature
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参考文献
Heinicke, Joachim
Journal of Organometallic Chemistry, 1989 , vol. 364, p. C17 - C21
反应条件
(i) Me2NCH2CH2NMe2, Et2O, (ii) /BRN= 605287/; Multistep reaction;
参考文献
Walborsky,H.M.; Ronman,P.
Journal of Organic Chemistry, 1978 , vol. 43, # 4 p. 731 - 734
反应条件
1: 38 percent / Me6Sn2 / benzene / 24 h / 80 °C / Irradiation
2: 85 percent / PCC, Celite / CH2Cl2 / Ambient temperature
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参考文献
Josien, Hubert; Curran, Dennis P.
Tetrahedron, 1997 , vol. 53, # 26 p. 8881 - 8886
参考文献
Hofmann,A.W.
Chemische Berichte, 1877 , vol. 10, p. 1095
参考文献
Hofmann,A.W.
Chemische Berichte, 1877 , vol. 10, p. 1095
反应条件
in benzene
under N2; evapn. under vac., residue redissolved in benzene, addn. of hexane, filtered out, rinsed with acetonitrile and ether, dried under vac., recrystn. (benzene/hexane);
参考文献
Ratliff, K. S.; DeLaet, D. L.; Gao, J.; Fanwick, P. E.; Kubiak, C. P.
Inorganic Chemistry, 1990 , vol. 29, p. 4022 - 4027
参考文献
Passerini; Bonciani
Gazzetta Chimica Italiana, 1931 , vol. 61, p. 959,960,963
参考文献
Ridi
Gazzetta Chimica Italiana, 1941 , vol. 71, p. 462,464
参考文献
Nef
Justus Liebigs Annalen der Chemie, 1892 , vol. 270, p. 281
Full Text Show Details
Hofmann,A.W.
Justus Liebigs Annalen der Chemie, 1867 , vol. 144, p. 118
