1197040-29-1合成路线 （共 99 条）
反应条件
in diethyl ether N2-atmosphere; molar ratio Cr:PhNC=1:1.2, stirring (room temp., overnight);; solvent removal (reduced pressure), chromy. (SiO2, ether/hexane=1:2, -10°C);;
参考文献
Journal of Organometallic Chemistry, , vol. 295, p. 51 - 62
反应条件
in diethyl ether N2-atmosphere; twofold excess of PhNC, stirring (room temp., overnight);; solvent removal (reduced pressure), chromy. (SiO2, ether/hexane=1:2, -10°C);;
参考文献
Journal of Organometallic Chemistry, , vol. 295, p. 51 - 62
反应条件
1: AgCl / -15 °C 2: CHCl3 / 6 h / Heating View Scheme
参考文献
Hegarty, Anthony F.; Chandler, Anne
Tetrahedron Letters, 1980 , vol. 21, p. 885 - 888
反应条件
N-iodo-succinimide; sodium azide; [14C]-Tetramethylammonium bromide in chloroform; water 1.) 0 deg C, 5 min, 2.) 0 deg C, 45 min;
参考文献
Collibee; Nakajima; Anselme
Journal of Organic Chemistry, 1995 , vol. 60, # 2 p. 468 - 469
反应条件
selenium unter Lichtausschluss;
参考文献
Lipp et al.
Monatshefte fuer Chemie, 1959 , vol. 90, p. 41,45
反应条件
sodium tris(acetoxy)borohydride T=-40 - 0°C; 7 h;
参考文献
Kiselyov, Alexander S.
Tetrahedron Letters, 2005 , vol. 46, # 26 p. 4487 - 4490
反应条件
byproducts: CO; prepn. from (CO)3NiC(CH3)2P(C6H5)3 and 11-fold excess of C6H5NC;;
参考文献
Diss. Heidelberg 1968
参考文献
Nef
Justus Liebigs Annalen der Chemie, 1892 , vol. 270, p. 281
参考文献
Nef
Justus Liebigs Annalen der Chemie, 1892 , vol. 270, p. 281
反应条件
hexamethyl-distannane in benzene
T=70°C; Irradiation; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Curran, Dennis P.; Ko, Sung-Bo; Josien, Hubert
Angewandte Chemie, 1995 , vol. 107, # 23/24 p. 2948 - 2950
