3,4-二甲氧基苯甲醛合成路线 （共 996 条）
反应条件
Fremy’s salt; anhydrous carbonate in ethanol; water 72 h; Mechanism;
参考文献
Tetrahedron Letters, , vol. 22, # 23 p. 2233 - 2236
反应条件
manganese triacetate in acetic acid 0.333333 h; Heating;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 44, # 12 p. 2218 - 2222
反应条件
sodium hydride; triphenylphosphine; zinc; NiCl2((PPh3)P)2 in toluene T=90 - 95°C; Ullmann-type coupling reaction; 12 h; Product distribution; Further Variations:Reagentsreaction time;
参考文献
Synlett, , # 10 p. 1527 - 1530
反应条件
sodium hydride; triphenylphosphine; zinc; NiCl2((PPh3)P)2 in toluene T=90 - 95°C; Ullmann-type coupling reaction; 4 h; Product distribution; Further Variations:Reagentsreaction time;
参考文献
Synlett, , # 10 p. 1527 - 1530
反应条件
1: 47.8 percent / toluene / 110 °C 2: 1.) Na, 2.) aq. oxalic acid / 1.) C2H5OH, 0 deg C to 5 deg C, 40 min, 2.) reflux View Scheme
参考文献
Synthetic Communications, , vol. 27, # 15 p. 2701 - 2707
反应条件
1: 96 percent / sodium borohydride / ethanol 2: 48 percent / lead tetraacetate / benzene / Heating View Scheme
参考文献
Synthetic Communications, , vol. 10, # 7 p. 573 - 580
反应条件
1: acetonitrile / 2 h / 80 °C 2: 1) AgCl, 2) rat liver enzymes / 1) methanol, 2) 37 deg C, 2 h, pH 7.5 View Scheme
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 45, # 3 p. 956 - 965
反应条件
trichlorophosphate T=100°C; durch Behandeln des Reaktionsprodukts mit kaltem Wasser;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 14, p. 166
反应条件
potassium hydroxide T=70 - 80°C; elektrolytische Oxydation an Bleidioxyd-Anode;
参考文献
Helvetica Chimica Acta, , vol. 8, p. 333
反应条件
ammonium cerium(IV) nitrate in acetonitrile 1.5 h; Heating;
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 25, p. 745
