3,4-二甲氧基苯甲醛合成路线 （共 996 条）
反应条件
formic acid; triethylamine in diethyl ether; ethanol; chloroform; water; Petroleum ether
参考文献
BIOGAL GYOGYSZERGYAR
Patent: EP578850 A1, 1994 ;
反应条件
1: 1) piperidine, 2) conc. H2SO4 / 1) pyridine
2: hydrogen / 5percent Pd/C / ethanol
View Scheme
参考文献
Brown; Blakemore; Durant; Emmett; Ganellin; Parsons; Rawlings; Walker
European Journal of Medicinal Chemistry, 1988 , vol. 23, # 1 p. 53 - 62
反应条件
ammonium acetate; sodium hydrogensulfite in ethanol; water
T=80°C; 0.5 h;
参考文献
Sangshetti, Jaiprakash N.; Kokare, Nagnnath D.; Kotharkar, Sandeep A.; Shinde, Devanand B.
Monatshefte fur Chemie, 2008 , vol. 139, # 2 p. 125 - 127
反应条件
ammonium acetate; sodium hydrogensulfite in ethanol; water
T=80°C; 0.833333 h;
参考文献
Sangshetti, Jaiprakash N.; Kokare, Nagnnath D.; Kotharkar, Sandeep A.; Shinde, Devanand B.
Monatshefte fur Chemie, 2008 , vol. 139, # 2 p. 125 - 127
反应条件
molybdenum oxide supported on silica in acetonitrile
T=80°C; 3 h;
参考文献
Bhosale, Sidhanath V.; Kalyankar, Mohan B.; Nalage, Santosh V.; Bhosale, Dattatry S.; Pandhare, Swati L.; Kotbagi, Trupti V.; Umbarkar, Shubhangi B.; Dongare, Mohan K.
Synthetic Communications, 2011 , vol. 41, # 5 p. 762 - 769
反应条件
molybdenum oxide supported on silica in acetonitrile
T=80°C; 3.2 h;
参考文献
Bhosale, Sidhanath V.; Kalyankar, Mohan B.; Nalage, Santosh V.; Bhosale, Dattatry S.; Pandhare, Swati L.; Kotbagi, Trupti V.; Umbarkar, Shubhangi B.; Dongare, Mohan K.
Synthetic Communications, 2011 , vol. 41, # 5 p. 762 - 769
反应条件
diethyl ether; sodium ethanolate
参考文献
Stobbe
Justus Liebigs Annalen der Chemie, 1911 , vol. 380, p. 77
反应条件
sodium hydride
1.) toluene, oil, 30 min, 2.) 60 deg C, 18 h; Multistep reaction;
参考文献
Boshoff, Philip R.; Perold, Guido W.
Journal of Chemical Research, Miniprint, 1986 , # 2 p. 735 - 745
反应条件
Reaktion ueber mehrere Stufen;
参考文献
Stobbe; Leuner
Justus Liebigs Annalen der Chemie, 1911 , vol. 380, p. 78
反应条件
Verseifen des Reaktionsproduktes mit kochendem Barytwasser;
参考文献
Stobbe; Leuner
Justus Liebigs Annalen der Chemie, 1911 , vol. 380, p. 76
