3,4-二甲氧基苯乙胺合成路线 （共 365 条）
参考文献
Pharmazie, , vol. 44, # 3 p. 215 - 218
反应条件
1: und Erwaermen des Reaktionsprodukts mit wss.Aethanol 2: formic acid / 210 °C / Erhitzen des Reaktionsprodukts in Toluol mit Phosphor(V)-oxid und Behandeln des danach erhaltenen Reaktionsprodukts mit wss.Natronlauge View Scheme
参考文献
Buck
Journal of the American Chemical Society, 1930 , vol. 52, p. 4119,4121
反应条件
1: Na2SO4 / 1,2-dichloro-ethane / 0.5 h / Heating 2: 1.) SOCl2, KI / 1.) 1,2-dichloroethane, room temp., 1 h, 2.) room temp., 3 h View Scheme
参考文献
Synthesis, , # 1 p. 59 - 61
反应条件
1: Na2SO4 / 1,2-dichloro-ethane / 0.5 h / Heating 2: 1.) SOCl2, KI / 1.) 1,2-dichloroethane, room temp., 1 h, 2.) room temp., 3 h View Scheme
参考文献
Venkov; Lukanov
Synthesis, 1989 , # 1 p. 59 - 61
参考文献
Pharmaceutical Chemistry Journal, , vol. 20, # 4 p. 259 - 264
Khimiko-Farmatsevticheskii Zhurnal, , vol. 20, # 4 p. 433 - 437
反应条件
1.1: 85 percent / 1 h / 110 °C 2.1: 85 percent / NaBH4 / methanol / 2 h / Heating 3.1: HOAc; CuSO4; NaCl / 0.5 h / 50 °C 3.2: 60 percent / AcOH / 6 h / 85 °C View Scheme
参考文献
Bian, Xiaoli; He, Langchong; Yang, Guangde
Bioorganic and Medicinal Chemistry Letters, 2006 , vol. 16, # 5 p. 1380 - 1383
反应条件
1: in ethanol T=25 - 30°C; 24 h; 2: With hydrogenchloride in ethyl acetate
参考文献
Bredikhina, Zemfira A.; Zakharychev, Dmitry V.; Gubaidullin, Aidar T.; Bredikhin, Alexander A.
Journal of Molecular Structure, 2009 , vol. 936, # 1-3 p. 171 - 176
反应条件
PPA in dichloromethane T=80°C; 3 h;
参考文献
Venkov, Atanas P.; Ivanov, Ilian I.
Tetrahedron, 1996 , vol. 52, # 37 p. 12299 - 12308
反应条件
1: Heating 2: phosphorous oxychloride / toluene / Heating View Scheme
参考文献
Bremner; Coban; Griffith; Groenewoud; Yates
Bioorganic and medicinal chemistry, 2000 , vol. 8, # 1 p. 201 - 214
参考文献
Venkov, Atanas P.; Ivanov, Ilian I.
Tetrahedron, 1996 , vol. 52, # 37 p. 12299 - 12308
