反应条件
in methanol; toluene under N2; soln. of Co complex in toluene treated with equimolar amt. ofP(OMe)3 at 0 °C, then dropwise added CH2Br2, stirred for 1 h, added pentane, filtered, dried in vac., NH4PF6 added, added MeOH, stirred for 10 min; added Et2O, filtered, recrystd. (acetone/Et2O); elem. anal.;
参考文献
Hofmann, L.; Werner, H.
Journal of Organometallic Chemistry, 1985 , vol. 289, p. 141 - 156
