in dichloromethane
soln. of P(OMe)3 was added to a stirred soln. of (Mo(H2CPz'2)(CO)2(π-allyl)Br); reaction was monitored by IR-spectroscopy (every 10 min);; evapn. of solvent (vac.); recrystn. from CH2Cl2/hexane;;
in dichloromethane
soln. of P(OMe)3 was added to a stirred soln. of (Mo(H2CPz'2)(CO)2Br2); reaction was monitored by IR-spectroscopy (every 10 min);; evapn. of solvent (vac.); recrystn. from CH2Cl2/hexane;;
