N,N-二甲基-间甲基苯胺合成路线 (共 64 条)
反应条件
tert.-butylhydroperoxide; tetra-(n-butyl)ammonium iodide in water; 1,2-dichloro-ethane
T=90°C; 10 h;
参考文献
Mai, Wen-Peng; Song, Ge; Yuan, Jin-Wei; Yang, Liang-Ru; Sun, Gang-Chun; Xiao, Yong-Mei; Mao, Pu; Qu, Ling-Bo
RSC Advances, 2013 , vol. 3, # 12 p. 3869 - 3872
反应条件
zinc(II) chloride
auf dem Wasserbade;
参考文献
Noelting
Chemische Berichte, 1901 , vol. 34, p. 825
Full Text Show Details
Fischer,O.
Chemische Berichte, 1880 , vol. 13, p. 808
反应条件
1: With tert-butyl methyl ether; nitric acid in tetrahydrofuran
T=0°C;
2: With sulfuric acid in dichloromethane
T=0°C; 1 h; Further stages. Title compound not separated from byproducts.;
参考文献
Zhang, Pingsheng; Cedilote, Miall; Cleary, Thomas P.; Pierce, Michael E.
Tetrahedron Letters, 2007 , vol. 48, # 49 p. 8659 - 8664
参考文献
Brady; Gibson
Journal of the Chemical Society, 1921 , vol. 119, p. 102
Full Text Show Details
Wurster; Riedel
Chemische Berichte, 1879 , vol. 12, p. 1797
参考文献
Brady; Gibson
Journal of the Chemical Society, 1921 , vol. 119, p. 102
Full Text Show Details
Wurster; Riedel
Chemische Berichte, 1879 , vol. 12, p. 1797
参考文献
Brady; Gibson
Journal of the Chemical Society, 1921 , vol. 119, p. 102
Full Text Show Details
Wurster; Riedel
Chemische Berichte, 1879 , vol. 12, p. 1797
反应条件
2: acetic acid / (nitration)
View Scheme
参考文献
Senning,A.
Acta Chemica Scandinavica (1947-1973), 1963 , vol. 17, # 9 p. 2570 - 2572
参考文献
Senning,A.
Acta Chemica Scandinavica (1947-1973), 1963 , vol. 17, # 9 p. 2570 - 2572
反应条件
phosphorus trichoride
T=127°C; und Verruehren des Reaktionsprodukts mit Natronaluge und Eis;
参考文献
Cassella and Co.
Patent: DE397813 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 14, p. 1409
参考文献
Newkome, George R.; Yuanjiao, Xia
Heterocycles, 1983 , vol. 20, # 6 p. 981 - 982