甲基4-甲氧基苯甲酸酯合成路线 (共 354 条)
反应条件
potassium carbonate in acetone 4 h; Inert atmosphereReflux;
参考文献
Ogura, Tetsuhiro; Usuki, Toyonobu
Tetrahedron, 2013 , vol. 69, # 13 p. 2807 - 2815
反应条件
sulfuric acid T=80 - 85°C; 16 h; Neat (no solvent);
参考文献
Rekha; Ramani, Modukuri V.; Ratnamala; Rupakalpana, Vempati; Subbaraju, Gottumukkala V.; Satyanarayana, Chava; Rao, C. Someswara
Organic Process Research and Development, 2009 , vol. 13, # 4 p. 769 - 773
反应条件
copper quinolate; tetra-(n-butyl)ammonium iodide in water; dimethyl sulfoxide T=120°C; 24 h;
参考文献
Zhu, Yan; Yan, Hong; Lu, Linhua; Liu, Defu; Rong, Guangwei; Mao, Jincheng
Journal of Organic Chemistry, 2013 , vol. 78, # 19 p. 9898 - 9905
反应条件
oxygen; palladium diacetate; zinc(II) chloride T=100°C; P=5700.38 Torr; 24 h;
参考文献
Wang, Azhong; Jiang, Huanfeng
Journal of the American Chemical Society, 2008 , vol. 130, # 15 p. 5030 - 5031
反应条件
sulfuric acid 4 h; Reflux;
参考文献
De Oliveira, Cledualdo Soares; Lira, Bruno Freitas; Falcao-Silva, Vivyanne Dos Santos; Siqueira-Junior, Jose Pinto; Barbosa-Filho, Jose Maria; De Athayde-Filho, Petronio Filgueiras
Molecules, 2012 , vol. 17, # 5 p. 5095 - 5107
反应条件
C57H43IP2Pd; triethylamine T=130°C; P=3750.38 Torr; 24 h; Autoclave;
参考文献
Kaganovsky, Luba; Gelman, Dmitri; Rueck-Braun, Karola
Journal of Organometallic Chemistry, 2010 , vol. 695, # 2 p. 260 - 266
反应条件
1: 1-bromo-4-methoxy-benzene With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 0.5 h; 2: N,N-dimethyl-formamide in tetrahydrofuran; hexane T=-78 - 20°C; 2 h; 3: methanol Further stages;
参考文献
Ushijima, Sousuke; Moriyama, Katsuhiko; Togo, Hideo
Tetrahedron, 2012 , vol. 68, # 24 p. 4701 - 4709
反应条件
CuF2 in dimethyl sulfoxide T=100°C; 12 h; Schlenk techniqueInert atmosphereGreen chemistry; Reagent/catalystTemperature;
参考文献
Li, Pan; Zhao, Jingjing; Lang, Rui; Xia, Chungu; Li, Fuwei
Tetrahedron Letters, 2014 , vol. 55, # 2 p. 390 - 393
反应条件
CuF2 in water; dimethyl sulfoxide T=120°C; 12 h; Schlenk techniqueInert atmosphereGreen chemistry;
参考文献
Li, Pan; Zhao, Jingjing; Lang, Rui; Xia, Chungu; Li, Fuwei
Tetrahedron Letters, 2014 , vol. 55, # 2 p. 390 - 393
反应条件
potassium hydroxide; iodine T=0°C; 2 h;
参考文献
Karade; Shirodkar; Dhoot; Waghmare
Journal of Chemical Research, 2005 , # 4 p. 274 - 276