甲基4-甲氧基苯甲酸酯合成路线 （共 354 条）
参考文献
Rosenthaler
Pharmaceutica Acta Helvetiae, 1937 , vol. 12, p. 8
反应条件
1: With potassium tert-butylate in toluene T=20°C; 1.16667 h; Cooling with ice; 2: With hydrogenchloride in water pH=~ 2;
参考文献
Dai Nippon Printing Co., Ltd.
Patent: EP2415840 A1, 2012 ;
Location in patent: Page/Page column 33-34 ;
反应条件
lithium chloride in N,N-dimethyl-formamide 0.166667 h; Microwave irradiation; chemoselective reaction;
参考文献
Wu, Xiao-Ai; Ying, Ping; Liu, Jun-Yang; Shen, Heng-Shui; Chen, Yue; He, Ling
Synthetic Communications, 2009 , vol. 39, # 19 p. 3459 - 3470
反应条件
1: ethyl bromoacetate With zinc in tetrahydrofuran T=50 - 55°C; 0.333333 h; 2: methyl 4-(N-tert-butoxycarbonyl-(5S)-methyl-(2S)-pyrrolidinylmethoxy)benzoate in tetrahydrofuran 20 h; Heating;
参考文献
Tetrahedron, , vol. 59, # 19 p. 3481 - 3485
反应条件
indium; iodine transesterification; 30 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 63, # 17 p. 6027 - 6028
反应条件
1: CH3BF3(1-)*H(1+)*C4H10O; N-bromosuccinmide / acetonitrile / 23 h / -10 - 20 °C / |Inert atmosphere 2: diisobutylaluminium hydride / tetrahydrofuran; hexane / 1 h / -78 - 0 °C / |Inert atmosphere View Scheme
参考文献
Ogura, Tetsuhiro; Usuki, Toyonobu
Tetrahedron, 2013 , vol. 69, # 13 p. 2807 - 2815
反应条件
1: 94.4 percent / LiAlH4 / diethyl ether / 4 h / Heating 2: 93.8 percent / SOCl2 / diethyl ether / 3 h / 20 °C 3: 4 h / Heating 4: NaOEt / dimethylformamide; ethanol / 3 h / 20 °C View Scheme
参考文献
Chen, Guoliang; Shan, Wei; Wu, Yingliang; Ren, Lixiang; Dong, Jinhua; Ji, Zhizhong
Chemical and Pharmaceutical Bulletin, 2005 , vol. 53, # 12 p. 1587 - 1590
反应条件
1: sodium hydride / toluene; mineral oil / 90 °C 2: hydrogenchloride / water / Reflux View Scheme
参考文献
Danel, Krzysztof S.; Uchacz, Tomasz; Karelus, Marcin
Arkivoc, 2011 , vol. 2011, # 9 p. 272 - 280
反应条件
tetraethylammonium p-toluenesulfonate Electrochemical reactionSn cathode; Pt anode; constant current 0.2 A; divided cell;
参考文献
Kise; Hirata; Ueda
Journal of Organic Chemistry, 2001 , vol. 66, # 3 p. 862 - 867
反应条件
lithium hexamethyldisilazane in tetrahydrofuran T=-78°C; 0.166667 h;
参考文献
Gissot, Arnaud; Volonterio, Alessandro; Zanda, Matteo
Journal of Organic Chemistry, 2005 , vol. 70, # 17 p. 6925 - 6928
