(1,5-环辛二烯)二氯化钯(II)合成路线 （共 29 条）
反应条件
in chloroform-d1 byproducts: CND-1,5; exchange reactions complete at 50°C in 43 h; various temp. and time various yields;
参考文献
Rettig,M.F.; Wing,R.M.; Wiger,G.R.
Journal of the American Chemical Society, 1981 , vol. 103, p. 2980
反应条件
in chloroform-d1 placed in 50°C bath for 42 h;
参考文献
Rettig,M.F.; Wing,R.M.; Wiger,G.R.
Journal of the American Chemical Society, 1981 , vol. 103, p. 2980
反应条件
in dichloromethane Pd compd. disolved in CH2Cl2, COD-1,5 added, standing for 24 h;
参考文献
Journal of the American Chemical Society, , vol. 103, p. 2980
反应条件
in water; acetone Kinetics; reaction in an aq. acetone soln. at 25°C; followed by UV and (1)H NMR;
参考文献
Inorganic Chemistry, , vol. 25, p. 243 - 244
反应条件
in diethyl ether byproducts: CH4, Ph3SiOH; inert atmosphere; dry HCl;
参考文献
Inorganica Chimica Acta, , vol. 294, # 2 p. 266 - 274
反应条件
in diethyl ether byproducts: CH4, Ph3SiOH; inert atmosphere; dry HCl;
参考文献
Inorganica Chimica Acta, , vol. 294, # 2 p. 266 - 274
反应条件
in acetonitrile-D3 byproducts: COD, ethene, ethane; Ar-atmosphere; in presence or absence of Et4Sn; further byproduct: Pd; not isolated, reaction followed by NMR spectroscopy;
参考文献
Canadian Journal of Chemistry, , vol. 74, # 11 p. 1990 - 1997
反应条件
in not given N2-atmosphere;
参考文献
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), , p. 1010 - 1016
反应条件
in dichloromethane-d2 byproducts: C4H4OO2(C(CH3)2CH(O)CH2O(C(CH3)2OCH2ClPd(COD); room temp.; not isolated, detected by NMR;
参考文献
Journal of Chemical Research, Synopses, , p. 98 - 99
反应条件
in dichloromethane under N2, addn. of complex in CH2Cl2 to soln. of ligand in CH2Cl2, stirred for 25°C for 2 h, white pptn.; evapd. under reduced press., addn. of toluene, heated under reflux for 4 h, pptn., filtered, dried in vac.;
参考文献
Broadwood-Strong, Gillian T. L.; Chaloner, Penny A.; Hitchcock, Peter B.
Polyhedron, 1993 , vol. 12, p. 721 - 730
