5-亚苄基-2,2-二甲基-1,3-二恶烷-4,6-二酮合成路线 （共 31 条）
反应条件
hydrogenchloride
1.) ether, THF;
参考文献
Ziegler, Frederick E.; Guenther, Thomas; Nelson, Richard V.
Synthetic Communications, 1980 , vol. 10, # 9 p. 661 - 666
反应条件
triethylamine in N,N-dimethyl-formamide
T=60°C; Inert atmosphere;
参考文献
Westerlich, Slawomir; Jagodzinski, Tadeusz S.
Arkivoc, 2010 , vol. 2010, # 11 p. 336 - 342
反应条件
1: 76.5 percent / sodium methoxide / tetrahydrofuran / 18 h / 0 - 15 °C
2: 80 percent / 2.) aq. HCl / 1.) ether, THF
View Scheme
参考文献
Ziegler, Frederick E.; Guenther, Thomas; Nelson, Richard V.
Synthetic Communications, 1980 , vol. 10, # 9 p. 661 - 666
反应条件
in water
T=75°C; 2 h;
参考文献
Le, Wen-Jun; Lu, Hong-Fei; Zhou, Jun-Tao; Cheng, He-Long; Gao, Yu-Hua
Tetrahedron Letters, 2013 , vol. 54, # 39 p. 5370 - 5373
反应条件
in acetonitrile
T=20°C; Knoevenagel condensation; 2 h;
参考文献
Wang, Qi-Fang; Hui, Li; Hou, Hong; Yan, Chao-Guo
Journal of Combinatorial Chemistry, 2010 , vol. 12, # 2 p. 260 - 265
反应条件
in acetonitrile
T=20°C; Knoevenagel condensation; 2 h;
参考文献
Wang, Qi-Fang; Hui, Li; Hou, Hong; Yan, Chao-Guo
Journal of Combinatorial Chemistry, 2010 , vol. 12, # 2 p. 260 - 265
反应条件
in acetonitrile
T=20°C; Knoevenagel condensation; 2 h;
参考文献
Wang, Qi-Fang; Hui, Li; Hou, Hong; Yan, Chao-Guo
Journal of Combinatorial Chemistry, 2010 , vol. 12, # 2 p. 260 - 265
反应条件
in acetonitrile
T=20°C; Knoevenagel condensation;
参考文献
Wang, Qi-Fang; Hui, Li; Hou, Hong; Yan, Chao-Guo
Journal of Combinatorial Chemistry, 2010 , vol. 12, # 2 p. 260 - 265
反应条件
in acetonitrile
T=20°C; Knoevenagel condensation; 2 h;
参考文献
Wang, Qi-Fang; Hui, Li; Hou, Hong; Yan, Chao-Guo
Journal of Combinatorial Chemistry, 2010 , vol. 12, # 2 p. 260 - 265
反应条件
in acetonitrile
T=20°C; Knoevenagel condensation;
参考文献
Wang, Qi-Fang; Hui, Li; Hou, Hong; Yan, Chao-Guo
Journal of Combinatorial Chemistry, 2010 , vol. 12, # 2 p. 260 - 265
