反应条件
1: di-isopropylamine, BuLi / tetrahydrofuran; hexane / 1.) -78 deg C, 1 h; 2.) room temp. 1 h 2: 2.) caesium fluoride / 1.) THF, -78 deg C, 1 h ; 2.) THF, -78 deg C, 8 h, room temp., 8 h 3: 95 percent / 10M HCl / tetrahydrofuran / 24 h / Ambient temperature View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 819 - 824
