1: N-bromosuccinmide; dibenzoyl peroxide / benzene / 0.33 h / Inert atmosphere; Photolysis 2: sodium azide; acetic acid / ethanol; water / 74 h / 4 °C 3: toluene / 15 h / Photolysis View Scheme
参考文献
Ranaweera, Ranaweera A. A. Upul; Zhao, Yu; Muthukrishnan, Sivaramakrishnan; Keller, Christopher; Gudmundsdottir, Anna D.
Australian Journal of Chemistry, 2010 , vol. 63, # 12 p. 1645 - 1655
1: N-bromosuccinmide; dibenzoyl peroxide / benzene / 0.33 h / Inert atmosphere; Photolysis 2: sodium azide; acetic acid / ethanol; water / 74 h / 4 °C 3: chloroform / Photolysis View Scheme
参考文献
Ranaweera, Ranaweera A. A. Upul; Zhao, Yu; Muthukrishnan, Sivaramakrishnan; Keller, Christopher; Gudmundsdottir, Anna D.
Australian Journal of Chemistry, 2010 , vol. 63, # 12 p. 1645 - 1655
1: N-bromosuccinmide; dibenzoyl peroxide / benzene / 20 h / Reflux 2: azide on Amberlite IRA-400 exchange resin / acetonitrile / 504 h 3: chloroform-d1 / 4 h / -77 °C / Photolysis; Inert atmosphere View Scheme
参考文献
Upul Ranaweera, Ranaweera A. A.; Sankaranarayanan, Jagadis; Casey, Lydia; Ault, Bruce S.; Gudmundsdottir, Anna D.
Journal of Organic Chemistry, 2011 , vol. 76, # 20 p. 8177 - 8188
1: N-bromosuccinmide; dibenzoyl peroxide / benzene / 20 h / Reflux 2: azide on Amberlite IRA-400 exchange resin / acetonitrile / 504 h 3: oxygen / toluene / 4 h / 24.84 °C / Photolysis View Scheme
参考文献
Upul Ranaweera, Ranaweera A. A.; Sankaranarayanan, Jagadis; Casey, Lydia; Ault, Bruce S.; Gudmundsdottir, Anna D.
Journal of Organic Chemistry, 2011 , vol. 76, # 20 p. 8177 - 8188