1: 2-phenoxyacetic acid With 1,1'-carbonyldiimidazole in dichloromethane; water
T=0 - 20°C; 0.5 h; Inert atmosphere;
2: O,N-dimethyl-hydroxylamine hydrochloride With triethylamine in dichloromethane; water
T=0 - 20°C; Inert atmosphere;
参考文献
NORTH CAROLINA STATE UNIVERSITY; LINDSEY, Jonathan S.; MASS, Olga
Patent: WO2013/62670 A2, 2013 ;
Location in patent: Page/Page column 79 ;
1: With 4-(N,N-dimethlyamino)pyridine in dichloromethane
T=0°C; 0.0833333 h; Inert atmosphere;
2: With dicyclohexyl-carbodiimide in dichloromethane
T=0 - 20°C; 18.5 h; Inert atmosphere;
参考文献
Rueda-Becerril, Montserrat; Chatalova Sazepin, Claire; Leung, Joe C. T.; Okbinoglu, Tulin; Kennepohl, Pierre; Paquin, Jean-Francois; Sammis, Glenn M.
Journal of the American Chemical Society, 2012 , vol. 134, # 9 p. 4026 - 4029
