反应条件
1: C15H18O2 With n-butyllithium; tetramethylpiperidine in tetrahydrofuran; hexane Decomposition; deketalization; 0.5 h; dry ice:2-propanol cooling; ice-water cooling; 2: acetic anhydride in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide; hexane Acetylation; 0.5 h; ice-water cooling;
参考文献
Noh, Taehee; Gan, Hong; Halfon, Sharon; Hrnjez, Bruce J.; Yang, Nien-Chu C.
Journal of the American Chemical Society, 1997 , vol. 119, # 32 p. 7470 - 7482