1: homo-neral diphenyl dithioacetal With n-butyllithium; N,N,N',N,-tetramethylethylenediamine in tetrahydrofuran; hexane
T=0°C; 0.5 h;
2: butyraldehyde in tetrahydrofuran; hexane
T=0 - 20°C;
参考文献
Grigorieva, N. Ya.; Tsiklauri, P. G.
Russian Chemical Bulletin, 2004 , vol. 53, # 3 p. 665 - 670
Izvestiya Akademi Nauk, Seriya Khimicheskaya, 2004 , # 3 p. 635 - 639
1: bis(phenylthio)methane With n-butyllithium in tetrahydrofuran; hexane
T=0°C; 0.75 h;
2: butyraldehyde in tetrahydrofuran; hexane
T=0 - 20°C;
参考文献
Grigorieva, N. Ya.; Tsiklauri, P. G.
Russian Chemical Bulletin, 2004 , vol. 53, # 3 p. 665 - 670
Izvestiya Akademi Nauk, Seriya Khimicheskaya, 2004 , # 3 p. 635 - 639
1: With sodium sulfate in chloroform
T=20°C; 24 h;
2: With sodium tris(acetoxy)borohydride in chloroform
T=20°C; 24 h;
3: With methanol in chloroform
T=20°C;
参考文献
CEREP
Patent: US2009/233910 A1, 2009 ;
Location in patent: Page/Page column 57-58 ;
US 20090233910 A1
