2,3-O-1,1-环己烷二基-D-呋喃核糖合成路线 （共 4 条）
反应条件
camphor-10-sulfonic acid 12 h;
参考文献
Fairbanks, Antony J.; Fleet, George W. J.
Tetrahedron, 1995 , vol. 51, # 13 p. 3881 - 3894
反应条件
1: 59 percent / pyridinium chlorochromate / CH2Cl2 / 16 h / Ambient temperature; or with pyridinium dichromate 2: 96 percent / aq. NaOH, aq. NaIO4 / dioxane / 0.17 h / 0 °C View Scheme
参考文献
Liu; Caperelli
Synthesis, 1991 , # 11 p. 933 - 934
反应条件
pyridinium chlorochromate in dichloromethane 16 h; Ambient temperatureor with pyridinium dichromate;
参考文献
Liu; Caperelli
Synthesis, 1991 , # 11 p. 933 - 934
反应条件
1.1: tetrahydrofuran / 12 h / -78 - 20 °C
2.1: sodium periodate / methanol; water / 1 h / 0 - 20 °C
3.1: tetrahydrofuran / 0 °C
4.1: Grubb's 2nd generation catalyst / dichloromethane / 20 °C
5.1: Dess-Martin periodane; sodium hydrogencarbonate / dichloromethane / 2 h
5.2: 0.5 h
View Scheme
参考文献
Deng, Lisheng; Zhang, Li; Yao, Yuan; Wang, Cong; Redell, Michele S.; Dong, Shuo; Song, Yongcheng
MedChemComm, 2013 , vol. 4, # 5 p. 822 - 826
